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GCMS calibration table for method 508SCAN, April 2002

Machine-extracted title · confidence 100%

Calibration table listing internal standards and response factors for GCMS analysis dated April 17, 2002.

NYC-WTC_000047769–000047771

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020417\0408REF2.D Vial: 6 Acq On : 17 Apr 2002 1:31 pm Operator: Nefliu Sample : 04/08 ref Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 18 09:09:53 2002 Quant Results File: 041702SCAN. RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Apr 17 08:01:11 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.61 202 12271838 19.67 ug/L 99 38) Pyrene 27.25 202 12895024 22.72 ug/L 100 39) Butylbenzylphthalate 29.60 149 5375136 21.14 ug/L 94 40) Benzo(a)anthracene 30.86 228 9688389 20.71 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.46 149 6988960 22.14 ug/L 97 42) Chrysene 30.96 228 10600069m 23.45 ug/L 44) Di-n-octylphthalate 33 . 32 149 8751626 13.89 ug/L 98 45) Benzo(b)fluoranthene 33.90 252 9975829 23.09 ug/L 94 46) Benzo(k)fluoranthene 33.90 252 10027963 19.89 ug/L 98 47) Benzo(a)pyrene 34.63 252 6332259m 15.38 ug/L 48) Indeno(1,2,3-cd)pyrene 37.50 276 4082251 14.29 ug/L 98 49) Dibenz(a,h)anthracene 37.62 278 5499546 21.50 ug/L 98 50) Benzo(g,h,i)perylene 38.25 276 5919677 21.04 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0408REF2.D 041702SCAN.M Thu Apr 18 09:10:39 2002 Page 2

NYC-WTC_000047770

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NYC-WTC_000047770Source: NYC Law Department, mirrored locally

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