GCMS calibration table for method 508SCAN, April 2002

2 2 K Quantitation Report (QT Reviewed) K O o 2 Data File C:\MSDCHEM\1\DATA\020417\0408REF2 . D Vial 6 co — o Acq On 17 Apr 2002 1:31 pm Operator Nefliu "0 I C O O Sample 04/08 ref Inst Instrumen O O O Mise Multiplr 1.00 o' MS Integration Params: EVENTS.E "0 o Quant Time: Apr 18 9:10 2002 Quant Results File: 041702SCAN.RES — 0 o Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) o Q C Title 508 Modified GC/MS scan 3 CD Last Update Wed Apr 17 08:01:11 2002 Response via Initial Calibration Abundance TIC 0408REF2 D

SB a & C 3500000 C Q CD C TO a TO C S TO CD “j TO 3 Z o s' go ।: । > ।‘ Q. 6 3000000 N CD V) c 2 Q

o o o c CD

2500000- ii Q g C 3 1 D 3 C D o D @ C )

2000000- 8s tn 5 £ | c CD C 0) D 0 o Q. § Q S$ S S z% I o <D § 2 0 a 2 P TO TO S 5 CD 2 TO

I c o Q c D

2 3 2 5 2 O

I E Q so' 6 £ TO 0)

4i8 So ! X § § f I 11 1500000- @ 0 c N 0) ( • c is C

1 9 22 a CD w @ III ll2 o a Q 0) 2 J IM o S 3 & & 2 88 C o C I o 8 & I 0) - Q

S & I 8 NE 0 ©o 33 8 838 2 2 g8 P8g Q o CD co

1 0 IM C 2 Co S2 1000000- 0 C or— — ~ 6b • 0 O a) CD T 2 CD Ea $5584g2 — C ‘t 2 o at 2 a Fil5 o‘1 N C I Q

« I8 0i 1 i 9 Q X 9 G

500000

j t TO X CD

0 A 1 4.. . a —___ — __

Time—> 4 00 6.00 8.00 10.00 12.00 14.00 16.00 18 00 20 00 22 00 24.00 26.00 28.00 30.00 32 00 34.00 36.00 38 00

0408REF2.D 041702SCAN.M Thu Apr 18 09:10:39 2002 Page 3