GCMS reference results for sample AE07972, April 2002

2 2 K Quantitation Report (QT Reviewed) - o o 2 Data File C:\MSDCHEM\1\DATA\020415\0404REF2.D Vial : 5 co — o Acq On 15 Apr 2002 2:00 pm Operator: Nefliu "0 1 C O o Sample 04/04 ref Inst Instrumen O O O Mise Multiplr: 1.00 o' MS Integration Params: EVENTS.E "0 o C Quant Time: Apr 16 11:05 2002 — co Quant Results File: 041202SCAN.RES 0 O o Method : C:\MSDCHEM\l\METHQDS\041202SCAN.M (Chemstation Integrator) Q C Title : 508 Modified GC/MS scan 3 CD Last Update : Tue Apr 16 11:14:47 2002 Response via : Initial Calibration Abundance TIC 0404REF2 D 3000000 o i c Q

2800000 C 2 C o 8 d> G 6 2600000 d c C 0) ( C

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1400000 Q 3 e = D if § 2 CD

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( C D c Q c i o D $8 2 C 2 1 5 R f S0 J D

28 1200000 in? 1 & l O

>1 i Q. o • o S &? &g8 Q (o C 8 a u. Q. c £ 1 2 1000000 = 8j 5 p CD

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ili, 185 O N 9 e £ & a o g s II o 6 4 d Q

11 -p 800000 % = 88t83g E0-0 "2% 2 O 8 ( No 0 -- 8 X a X 3 § 1 I $O

600000 I & 12g2 X CD cP di §2 I Q ( f — 8 V)

C 400000' I § a 6 CD c

I 200000

Time—> 0 4 00 6.00 8.00 10.00 12.00 1 14 00 1

16.00 18.00 20.00 22 00 24.00 26 00 28.00 30 00 L 32.00 — 34.00 36 00 38 00

0404REF2 .D 041202SCAN.M Wed Apr 17 14:27:40 2002 Page 3