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GCMS calibration results for volatile organics, April 2002

Machine-extracted title · confidence 100%

Calibration data report for GCMS analysis of volatile organic compounds in sample AE08260 from April 2002.

NYC-WTC_000048256–000048259

Folder label: “GCMS X 4/9/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\020417\0417C4.D Vial: 2 Acq On : 17 Apr 2002 9:49 am Operator: Nefliu Sample : CCV Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 17 10:39:13 2002 Quant Results File: 041702SCAN. RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Apr 17 08:01:11 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.63 202 39232410 75.58 ug/L 97 38) Pyrene 27.27 202 40574853 86.19 ug/L 99 39) Butylbenzylphthalate 29.61 149 19615872 93.01 ug/L 96 40) Benzo(a)anthracene 30.87 228 32065261 82.62 ug/L 98 41) Bis(2-ethylhexyl)phthalate 31.47 149 25850431 98.70 ug/L 97 42) Chrysene 30.98 228 31134207m 83.04 ug/L 44) Di-n-octylphthalate 33.33 149 42862761 78.31 ug/L 98 45) Benzo(b)fluoranthene 33.85 252 29273510 77.98 ug/L 96 46) Benzo(k)fluoranthene 33.93 252 30751858 70.21 ug/L 96 47) Benzo(a)pyrene 34.66 252 26436209 73.92 ug/L 96 48) Indeno(1,2,3-cd)pyrene 37.53 276 19852473 80.00 ug/L 99 49) Dibenz(a,h)anthracene 37.65 278 20140984 90.61 ug/L 99 50) Benzo(g,h,i)perylene 38.30 276 20428850 83.56 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0417C4.D 041702SCAN.M Thu Apr 18 08:51:46 2002 Page 2

NYC-WTC_000048258

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NYC-WTC_000048258Source: NYC Law Department, mirrored locally

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