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GCMS reference analysis results for sample AE08251, April 2002

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Laboratory report of GCMS reference analysis for sample AE08251 conducted on April 17, 2002, showing recovery percentages for target compounds.

NYC-WTC_000047752–000047756

Folder label: “GCMS X 4/8/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\1\DATA\020417\0408REF1.D Vial: 5 Acq On : 17 Apr 2002 12:41 pm Operator: Nefliu Sample : 04/08 ref Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 17 13:36:37 2002 Quant Results File: 041702SCAN.RE

Quant Method : C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Last Update : Wed Apr 17 08:01:11 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

36) Fluoroanthene 26.61 202 11842334 20.06 ug/L 100 38) Pyrene 27.25 202 12477658 22.66 ug/L 99 39) Butylbenzylphthalate 29.60 149 5384545 21.82 ug/L 94 40) Benzo(a)anthracene 30.86 228 9357268 20.61 ug/L 99 41) Bis(2-ethylhexyl)phthalate 31.46 149 7112491 23.21 ug/L 98 42) Chrysene 30.96 228 10206924m 23.27 ug/L 44) Di-n-octylphthalate 33.32 149 9092462 14.51 ug/L 98 45) Benzo(b)fluoranthene 33.83 252 8251842m 19.21 ug/L 46) Benzo(k)fluoranthene 33.90 252 9815094 19.58 ug/L 97 47) Benzo(a)pyrene 34.63 252 6267096m 15.31 ug/L 48) Indeno(1,2,3-cd)pyrene 37.49 276 4363890 15.37 ug/L 98 49) Dibenz(a,h)anthracene 37.62 278 5808511 22.83 ug/L 100 50) Benzo(g,h,i)perylene 38.25 276 6138199 21.94 ug/L 99

(#) = qualifier out of range (m) = manual integration (+) = signals summed 0408REF1.D 04 1702SCAN.M Thu Apr 18 09:09:47 2002 Page 2

NYC-WTC_000047755

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NYC-WTC_000047755Source: NYC Law Department, mirrored locally

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