GCMS reference analysis results for sample AE08251, April 2002

z Quantitation Report (QT Reviewed) 2 - - o o 2 Data File C:\MSDCHEM\l\DATA\020417\0408REFl.D Vial 5 co — I o Acq On 17 Apr 2002 12:41 pm Operator Nefliu “0 O O Sample 04/08 ref Inst Instrumen C O 8 Mise Multiplr 1.00 o' “O MS Integration Params: EVENTS.E o — — CH, Quant Time: Apr 17 13:37 2002 Quant Results File: 041702SCAN.RES 0 0)1 o Method C:\MSDCHEM\1\METHODS\041702SCAN.M (Chemstation Integrator) oQ C Title 508 Modified GC/MS scan 3 Last Update Wed Apr 17 08:01:11 2002 CD

Response via Initial Calibration Abundance TIC: 0408REF1 D

3400000 o 3200000 o & 6 C

3000000 s O) I c re d

( G d o C 2800000 I ।: '2 ') ।: 0 2

a o 2600000 o

5 2400000 Q C | O D 2200000- D a 25 fl 0 5 8 3 a c Q re a 2000000 © 2 a Q

1 re

z D D re CL a ce i O c are re re a D Q d C fa 1800000 ( re

3 2 2> i C D 2 o % 2 i 6 - re 3 n re S 2 teg O g 1600000 c E G 1 3 IS * I c Ere o

1& 9 if N c

1400000 re

a 2al 2899 2 c g3 re re 9 C 29 re o I re re ar — 2 C o J 6 CM 1 z& 8 M o 0 8 3 ii& 8 c re a £ re

1200000 ® 298 8 6 f Hi 2 5.2 = S C11 i o 3( 9 re CD re o g g (y re

fl 8 °o N CD

J re 2 o 1000000 88182‘* 2 8 28 CM C o 6 CD T • I © Q C o re 800000 E re tS s S’ 51 8 C c

600000 o 5 0

s 8 mo C

I C re x U 0) 400000 C

200000

0-—— LL UL I 1 Time-> 4.00 6.00 8 00 10.00 12.00 14.00 16.00 18.00 20 00 22.00 24.00 26.00 28.00 30.00 32.00 34.00 36.00 38.00

0408REF1.D 04 1702SCAN . M Thu Apr 18 09:09:47 2002 Page 3