GCMS reference standard results for sample AE07978, April 2002

z 2 K Quantitation Report (QT Reviewed) - o 5 o 2 Data File C:\MSDCHEM\1\DATA\020415\0405REF1.D Vial : 6 co — o Acq On 15 Apr 2002 2:50 pm Operator: Nefliu "0 I o Sample C o 04/05 ref Inst : Instrumen O o o Mise Multiplr: 1.00 o' o MS Integration Params: EVENTS.E "0 o o Quant Time: Apr 16 11:07 2002 Quant Results File: 041202SCAN.RES — CD 0 o o Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Q C Title 508 Modified GC/MS scan 3 CD Last Update Tue Apr 16 11:14:47 2002 3 Response via Initial Calibration Abundance TIC 0405REF1 D 3200000 o C CD C Q 3000000 C re d I a re (2 o 2800000 d C C <d Q ore 2600000' 8 ' J ।: Z ।) । j 3 2400000 <D C ® N

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2000000 5 3 t CD & C 1800000 CD C P4 re a 5 D 3 D o A D 1600000 > .2 a 2 8 i a

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g8 Q 3D Q .5 z 89 CL9 Q J re 1400000 80s £ @ Q

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8 2 2 2 _E Q : ® a© JEC- _ 2 — Q 2 C re d’o’ E25S $82m o s re o o I 28 8 if (D

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@ 288 2 & 58 Q

siiJ 1000000 2232 220 a 516 9 48 ill 0 a o I C 1 *g $ x 3 &re o re

800000 Q C 85g% 85to. 32 ( &2 i 8 o

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600000 E re d $52 c 2 ( ! t5 t 2 O X N X I9 m§ 400000

200000 1 Time-> 0' 4.00 6 00 8.00 JU 10 00 UL 12.00 ULL 14 00 L 16 00 JU —U 18 00 20 00 ".A... I, U 22 00 24 00 26.00 28 00 30 00 32.00 ill........ 34 00 36 00 38 00

0405REF1.D 041202SCAN.M Wed Apr 17 14:28:01 2002 Page 3