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GCMS calibration table for method GCMS0412, April 2002

Machine-extracted title · confidence 100%

Calibration table listing internal standards and response factors for GCMS analysis dated April 16, 2002.

NYC-WTC_000047701–000047714

Folder label: “GCMS X 4/4/02 A 4/12/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1102\8016.D Vial: 22 Acq On : 12 Apr 2002 11:02 am Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.175 227 232 241 rBV2 23502 50024 1.42% 0.283% 2 12.225 777 782 798 rVB 1035621 2438134 69.10% 13.771% 3 14.061 977 982 993 rBV 151819 296083 8.39% 1.672% 4 14.832 1060 1066 1071 rVB 60098 120271 3.41% 0.679% 5 15.860 1172 1178 1194 rBV 1471822 3133759 88.81% 17.700%

6 21.166 1749 1756 1769 rBV 1714468 3528620 100.00% 19.930% 7 23.305 1982 1989 1995 rVB 179573 353823 10.03% 1.998% 8 25.609 2233 2240 2251 rBV 1614662 3378279 95.74% 19.081% 9 27.345 2421 2429 2436 rBV2 31614 80803 2.29% 0.456% 10 27.574 2449 2454 2463 rVB 62093 117119 3.32% 0.661%

11 29.713 2683 2687 2698 rBV2 28703 83969 2.38% 0.474% 12 33.661 3110 3117 3132 rBV2 1039257 2332481 66.10% 13.174% 13 37.893 3569 3578 3594 rBV2 511300 1543909 43.75% 8.720% 14 39.839 3782 3790 3800 rBV5 49323 183983 5.21% 1.039% 15 40.463 3854 3858 3869 rVB9 17676 63959 1.81% 0.361%

Sum of corrected areas: 17705216

8016.D GCMS0412.M Tue Apr 16 12:08:02 2002

NYC-WTC_000047704

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NYC-WTC_000047704Source: NYC Law Department, mirrored locally

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