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GCMS calibration table and instrument parameters, Apr 2002

Machine-extracted title · confidence 90%

Instrument calibration records and method parameters for GCMS analysis of polycyclic aromatic hydrocarbons.

NYC-WTC_000048583–000048597

Folder label: “GCMS X 4/10/02 A 4/15/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C : \HPCHEM\ 1 \DATA\APR12 02 \8481.D Vial: 26 Acq On : 16 Apr 2002 9:08 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 5.759 75 78 85 rBV 63417 128312 3.00% 0.540% 2 7.155 226 230 248 rBV 166559 416617 9.74% 1.754% 3 8.201 340 344 374 rVB 565547 1386194 32.40% 5.835% 4 12.231 777 783 800 rVB 1179741 2861464 66.88% 12.046% 5 13.911 960 966 971 rBV 32451 66059 1.54% 0.278%

6 14.829 1060 1066 1071 rW 248993 491423 11.49% 2.069% 7 15.013 1079 1086 1090 rBV5 14635 49180 1.15% 0.207% 8 15.169 1099 1103 1114 rVB2 22541 59279 1.39% 0.250% 9 15.867 1172 1179 1195 rW 1828158 3921036 91.65% 16.506% 10 17.675 1371 1376 1382 rVB 45293 84546 1.98% 0.356%

11 21.173 1750 1757 1773 rBV 1961441 4278411 100.00% 18.011% 12 23.303 1983 1989 1996 rBV 187354 386506 9.03% 1.627% 13 25.607 2233 2240 2252 rBV2 1905018 4073061 95.20% 17.146% 14 25.754 2252 2256 2268 rVB 14807 47239 1.10% 0.199% 15 33.667 3111 3118 3136 rBV2 1313629 3045765 71.19% 12.822%

16 37.909 3570 3580 3603 rBV2 780524 2459909 57.50% 10.355%

Sum of corrected areas: 23755001

8481.D GCMS0412.M Wed Apr 17 09:49:03 2002

NYC-WTC_000048586

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NYC-WTC_000048586Source: NYC Law Department, mirrored locally

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