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GCMS analysis results for sample AE06453, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039560–000039573

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039565
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\APR1702\6453.D Vial: 11 Acq On : 17 Apr 2002 6:00 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.101 328 333 346 rBV 182259 486100 14.34% 2.911% 2 8.248 346 349 360 rVB 17983 57569 1.70% 0.345% 3 12.214 775 781 792 rVB 848519 2117107 62.43% 12.679% 4 14.812 1059 1064 1070 rBV 42333 82183 2.42% 0.492% 5 15.840 1171 1176 1191 rBV 1375800 2875391 84.80% 17.220%

6 17.970 1402 1408 1413 rVB2 37060 72979 2.15% 0.437% 7 20.798 1708 1716 1721 rBV 24274 46896 1.38% 0.281% 8 21.147 1748 1754 1767 rBV 1716760 3390943 100.00% 20.308% 9 25.590 2231 2238 2248 rBV 1534072 3160649 93.21% 18.929% 10 27.554 2446 2452 2460 rVB 19176 35526 1.05% 0.213%

11 30.657 2785 2790 2795 rBV 248356 474945 14.01% 2.844% 12 33.641 3108 3115 3129 rBV2 968799 2199163 64.85% 13.170% 13 37.864 3567 3575 3593 rBV2 545105 1636900 48.27% 9.803% 14 38.488 3631 3643 3644 rBV3 16221 61428 1.81% 0.368%

Sum of corrected areas: 16697779

6453.D GCMS0412.M Thu Apr 18 09:12:47 2002

NYC-WTC_000039565

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NYC-WTC_000039565Source: NYC Law Department, mirrored locally

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