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GCMS analysis results for sample AE06454, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039574–000039587

Folder label: “GCMS X 3/19/02 A 4/17/02

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Scanned page image, NYC-WTC_000039579
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR1702\6454.D Vial: 12 Acq On : 17 Apr 2002 6:59 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.105 329 333 344 rBV 80216 231216 7.11% 1.464% 2 12.209 775 780 797 rVB 918219 2343243 72.08% 14.839% 3 14.807 1059 1063 1068 rBV 29715 56883 1.75% 0.360% 4 15.844 1170 1176 1193 rBV 1453947 2932737 90.22% 18.572% 5 17.965 1401 1407 1412 rBV2 37067 74610 2.30% 0.472%

6 20.801 1710 1716 1721 rBV 26546 49840 1.53% 0.316% 7 21.150 1747 1754 1767 rBV 1595033 3250705 100.00% 20.586% 8 23.326 1986 1991 1995 rBV2 18492 36015 1.11% 0.228% 9 25.584 2231 2237 2248 rW2 1439938 2985484 91.84% 18.906% 10 30.661 2785 2790 2796 rVB 203445 383271 11.79% 2.427%

11 33.635 3107 3114 3131 rBV2 829913 1918364 59.01% 12.149% 12 33.856 3133 3138 3147 rVB 43830 94930 2.92% 0.601% 13 37.307 3509 3514 3524 rVB4 12724 40595 1.25% 0.257% 14 37.867 3567 3575 3588 rBV2 486128 1392924 42.85% 8.821%

Sum of corrected areas: 15790817

6454.D GCMS0412.M Thu Apr 18 09:13:15 2002

NYC-WTC_000039579

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NYC-WTC_000039579Source: NYC Law Department, mirrored locally

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