TCLP calibration table review document, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\APR1702\8209.D Vial: 20 Acq On : 18 Apr 2002 2:46 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.209 775 780 795 rBV 1859936 4578545 72.71% 14.615% 2 15.845 1170 1176 1193 rBV 2725073 5685104 90.28% 18.147% 3 21.151 1747 1754 1769 rBV 3057326 6297196 100.00% 20.101% 4 23.281 1977 1986 1991 rBV 135437 272064 4.32% 0.868% 5 25.594 2231 2238 2248 rBV2 2796565 5960949 94.66% 19.028%

6 33.645 3107 3115 3134 rBV2 1917936 4349046 69.06% 13.883% 7 37.308 3509 3514 3524 rVB2 26952 82855 1.32% 0.264% 8 37.877 3567 3576 3590 rBV2 1097833 3285180 52.17% 10.487% 9 38.511 3629 3645 3664 rBV4 47507 467757 7.43% 1.493% 10 38.749 3665 3671 3682 rVB2 38533 159917 2.54% 0.510%

11 40.494 3852 3861 3873 rBV4 18750 90923 1.44% 0.290% 12 44.349 4265 4281 4282 rBV5 17064 97734 1.55% 0.312%

Sum of corrected areas: 31327270

8209.D GCMS0412.M Thu Apr 18 14:11:03 2002

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