Laboratory report documenting GCMS analysis of environmental sample AE07628 conducted on April 9, 2002.
NYC-WTC_000047245–000047255Folder label: “GCMS X 4/2/02 A 4/3/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\020403\07628.D Vial: 19 Acq On 4 Apr 2002 1:43 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Glaucine Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T. 14.69 0.21 ug/1 180235 Naphthalene-d8 15.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Glaucine 355 C21H25NO4 000475-81-0 3 2 6H-Dibenzo[a,g]quinolizine, 5,8,... 355 C21H25NO4 002934-97-6 3 3 Morphinan-6-one, 3,4-dimethoxy-N... 355 C22H29NO3 1000126-19-3 3 4 5H-Isoindolo[1,2-b][3]benzazepin... 355 C20H21NO5 055228-79-0 3 Abundance Scan 1976 (14.689 min): 07628.D (-1967) (-) m/z 73.10 100.00% 73
267 355 5000
■ ■ i 1 1 1 ' i 1 1 ■ 1 1 1 1 ' 1 i ' 1 14.40 14.60 14.80 15.00 0 ......... 40..................................................... m/z 355.00 51.04% u'1111 ■ " 11 ■' " r 111 r 11' i11,11"1'111111" 111 1’4’11 " " 1 I "" I < 1 1 1 11' 111 i! ! 11 n 111 i i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #103470: Glaucine 355
5000 ' 1 i 1 ■ ■ ' i ■ ■ • i ■ ■ ■ ■ i ■ ■ 14.40 14.60 14.80 15.00 m/ z 267.00 50.88% 281297 0 18 44 76 ' ‘‘i ' ■ ' ■ i 1 ■ 1 ' i ■ ' " i 97 118 140 TTTTTT 192178195211/ 238.,265.4.44.* n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #128845: 6H-Dibenzo[a,g]quinolizine, 5,8,13,13a-tetrahydro... 355 • > i ■ ■ ■ ■ । ■ ■ i ■ ■ > ■ i ■ • 149 14.40 14.60 14.80 15.00 5000 m/z 356.00 22.06% 165 190 324 77 104121
m/z-> Or ...44*44* +4>1.1 ITT i*h , 1* 206222238 HH;3 rum ira, ITi264280 T 4 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 308 1’’
Abundance #103465: Morphinan-6-one, 3,4-dimethoxy-N-cyclopropylmethyl- 355 14.40 14.60 14.80 15.00 m/ z 40.10 0.17% 204 314 5000
55 — 71 99 , 227 256. /z-> 115 141157 176 O- - mttrTpf TTTtr I 272
20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 2944 14.40 14.60 14.80 15.00
07628.D SCAN020403.M Thu Apr 04 10:36:31 2002 Page 6
NYC-WTC_000047254
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NYC-WTC_000047452
Technical documentation listing GC/MS method parameters and internal standard data for analysis performed in early April 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047463
Laboratory report detailing GCMS analysis of sample AE07768 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047216
Laboratory results for unknown compounds and surrogate recovery in sample AE07569 analyzed on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047389
Laboratory report documenting GCMS analysis of environmental sample AE07516 conducted on April 11, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047333
Laboratory report documenting GCMS analysis of environmental sample AE07511 conducted on April 11, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047377
Laboratory report documenting GCMS analysis of environmental sample AE07515 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047402
Laboratory report documenting GCMS analysis of environmental sample AE07518 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047256
Laboratory report documenting GCMS analysis of environmental sample AE07630 conducted on April 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047277
Laboratory report documenting GCMS analysis of environmental sample AE07632 conducted on April 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047355
Laboratory report documenting GCMS analysis of environmental sample AE07513 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047493
Laboratory report detailing GCMS analysis of sample AE07772 conducted on April 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047344
Laboratory report documenting GCMS analysis of environmental sample AE07512 conducted on April 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000047156
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated April 2-3 2002.
Filed in the same folder
NYC-WTC_000047157
Header page from a DEP laboratory data file containing sample identification and processing metadata from early April 2002.
Filed in the same folder
NYC-WTC_000047159
Laboratory results for volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.
Filed in the same folder
NYC-WTC_000047177
Laboratory report showing non-detect levels of volatile organic compounds in a GCMS blank sample analyzed on April 2-3, 2002.
Filed in the same folder
NYC-WTC_000047181
Calibration data report for GCMS analysis of volatile organic compounds performed on April 2-3, 2002.
Filed in the same folder