GCMS analysis results for sample AE07628, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\1\DATA\020403\07628.D Vial: 19 Acq On 4 Apr 2002 1:43 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Propanoyl chloride, 2-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

4.54 0.21 ug/1 138260 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Propanoyl chloride, 2-methyl- 106 C4H7C10 000079-30-1 2 2 Butane, 86 2,2-dimethyl- C6H14 000075-83-2 2 3 Propanoic acid, 2-methyl-, 2-eth... 286 C16H30O4 074367-30-9 2 4 1-Hexene, 4,5-dimethyl- 112 C8H16 016106-59-5 2 Abundance Scan 248 (4.536 min): 07628. D (-242) (-) m/z 43.10 100.00% 43 71

5000 55

4.20 4.40 4 4.60 1 1 i ■ ■ ■ ■ i 4.80 oW ■ i ■ ■' ■ i ■ ■ ■ ■ । ■11 '1111'11' ।'1 ■r । ■ ■ ■ ■ । • • ■' । > 111 ■ ■ । । ■ 11 > । > > 11'' 11 • ■ ■ ■ । ■ m/z 71.10 77.42% /z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #4446: Propanoyl chloride, 2-methyl- 43 71 5000 27 ' 1 1 1 ' 1 1 i 1 ■ । 1 ' ' ' । ■ 1 । 4.20 4.40 4.60 4.80 m/z 41.10 73.20% 15 ii ' 0 4 35 1 ,1--+r , 80 1ITTI ' 91 106 I '' " . ....... n/z-> 10 20 30) 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #109627: Butane, 2,2-dimethyl- 43 57 ' IIt 1 ' 1 1 1 1 TTI ‘ II 71 4.20 4.40 4.60 4.80 5000 m/ z 69.10 55.93% 29

o1 TTTTITpr+ -P TT +111,80 i ■ ■' ■ । i'''' i1' ■ i ■ ■'11'1 " i'' m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #6344: Propanoic acid, 2-methyl-, 2-ethyl-1-propyl-1,3-pro... 43 4.20 4.40 4.60 4.80 m/z 55.00 31.75% 71 5000 55

81 89 I'M A. mull,, a , । I; 110 127 143 155 o 11 ITT 11111 M 11 i ‘ ■ ■ * । ■ ■ I'1 1 1 1 [ 1 1 l'1 | 1 1 1 1 | I ' 1 I | ' ' ■ 1 । 1 1 ■ 1 i 1 1 ' 1 i ‘tl 1 i 1 1 1 1 । m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 4.20 4.40 4.60 4.80

07628.D SCAN020403.M Thu Apr 04 10:36:29 2002 Page 5

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