GCMS calibration results for volatile organics, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\020403\0403C3.D Vial: 9 Acq On 3 Apr 2002 4:25 pm Operator: Nefliu Sample ccvl Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: EVENTS.E Quant Time: Apr 05 09:08:29 2002 Quant Results File: SCAN020403.RE

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Last Update : Fri Apr 05 09:08:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN1

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 10.67 152 2684943 20.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 10274549 20.00 ug/1 0.01 17) Acenaphthene-diO 23.67 164 5585512 20.00 ug/1 0.00 31) Phenanthrene-diO 30.90 188 9408072 20.00 ug/1 0.00 39) Chrysene-dl2 39.11 240 9208989 20.00 ug/1 0.00 45) Perylene-dl2 42.31 264 5749674 20.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 0.00 207 Od 0.00 ug/1 Spiked Amount 5.000 Recovery = 0.00%

Target Compounds 2) N-nitrosodimethylamine 3.55 74 1717002 11.4' 31.5 Qvalue100 23.09 ug/1 3) bis(2-Chloroethyl)ether 9.96 93 3854279 27.54 ug/1 100 4) 1.3-Dichlorbenzene 10.42 146 4963909 25.78 ug/1 100 5) 1,4-Dichlorobenzene 10.73 146 5025384 25.75 ug/1 100 6) 1,2-Dichlorobenzene 11.25 146 4732381 25.68 ug/1 100 7) 2,2 ' oxybis(1-Chloropropane 12.04 45 2762289 29.58 ug/1 100 8) N-Nitroso-di-n-propylamine 12.55 43 2158149 27.61 ug/1 100 9) Hexachloroethane 12.52 119 1631071 26.87 ug/1 100 11) Nitrobenzene 12.96 77 4004786 27.75 ug/1 100 12) Isophorone 14.04 82 6775987 25.50 ug/1 100 13) bis(2-Chloroethoxy) methan 15.27 93 4592688 26.33 ug/1 100 14) 1,2,4-Trichlorobenzene 15.63 180 4018432 24.72 ug/1 100 15) Naphthalene 15.87 128 12729595 25.86 ug/1 100 16) Hexachlorobutadiene 16.63 225 2212101 24.24 ug/1 100 18) Hexachlorocyclopentadiene 19.80 237 1432199 28.86 ug/1 100 19) 2-Chloronaphthalene 21.16 162 7894313 25.76 ug/1 100 20) Acenaphthylene 22.97 152 10935524 25.55 ug/1 100 21) Dimethyl phthalate 23.08 163 8341876 25.14 ug/1 100 22) 2,6-Dinitrotoluene 23.19 77 410781 29.43 ug/1 100 23) Acenaphthene 23.81 153 8012149 25.93 ug/1 100 24) 2,4-Dinitrotoluene 24.95 165 1672969 23.47 ug/1 100 25) Fluorene 26.22 166 9118344 25.93 ug/1 100 26) Diethyl phthalate 26.44 149 8146769 25.51 ug/1 100 27) 4-Chlorophenyl-phenylether 26.55 204 4396462 25.80 ug/1 100 29) N-Nitrosodiphenylamine 27.16 168 3380592 25.94 ug/1 100 30) Azobenzene 27.25 77 8207034m 26.61 ug11 32) Hexachlorobenzene 28.80 284 3304072 25.23 ug/1 100 33) 4-Bromophenyl-phenylether 28.90 248 2733219 25.59 ug/1 100 34) Phenanthrene 31.01 178 13356496 25.75 ug/1 100 35) Anthracene 31.24 178 12979406 25.60 ug/1 100

(#) = qualifier out of range (m) = manual integration 0403C3.D SCAN020403.M Fri Apr 05 09:09:28 2002 Page 1

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