GCMS analysis report, sample AE07520, April 2002

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Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020403\0402LB.D vial: 10 Acq On 3 Apr 2002 5:21 pm Operator: Nefliu Sample 04/02 lab bik Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 7 IH-Pyrrolo[2,3-c]pyridine-3... Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 41.63 0.27 ug/1 200646 Perylene-dl2 42.30

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 IH-Pyrrolo[2,3-c]pyridine-3-prop... 222 C11H14N2O3 032682-61-4 7 2 4-isoxazolecarboxylic acid, 2,3-... 281 C17H15NO3 117644-85-6 7 3 3,7-Diamino-5H-dibenzo[a,d]cyclo... 222 C15H14N2 1000227-39-5 5 4 Ethenetricarbonitrile, 2,3-xylid... 222 C13H10N4 023957-66-6 5 Abundance Scan 6561 (41.629 min): 0402LB.D (-6557) (-) m/z 222.00 100.00% 212 147 5000 281 355 i > ■ ■ ■ i ■ ■ i ■ ■ ' ■ i ■ ' 40 41.20 41.40 41.60 41.80 42.00 0 1" " I' " 111 i ■'11111ITI" 11111111111111111 ' । >> 1111 m/z 147.10 62.73% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #88182:1 H-Pyrrolo[2,3-c]pyridine-3-propanoic acid, 5(4H)-... 212 149

5000 106 TUT I ' 1 ' ' I ' ' ' ■ I ' r 41.20 41.40 41.60 41.80 42.00 41 57 m k m/z 221.10 55.99% l i 83 121 191 0 —++--4A—4, 1 , R 1 . . । r i । । pt i । । । । । । । । । । । । । । । । । । 1 । । 1 । । । । । । ■ । । ■ । ।

■n/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #88042: 4-Isoxazolecarboxylic acid, 2,3-dihydro-2,3-diphen... 212 77 194 IIT ’t" I ' ' ■ 118 41.20 41.40 41.60 41.80 42.00 m/z 207.00 51.89%

A 5000 281

/z-> Abundance 0'' । " ।' 11 20 40 — m 252 m 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #88180: 3,7-Diamino-5H-dibenzo[a,d]cycloheptene 212 I'1'11 11' ‘ I T‘

.A 41.20 41.40 41.60 41.80 42.00 m/z 355.00 33.00% 5000

47 88 । 111 165 193 | A 0 111111 m | r 63 1 139 - i ■ 1* '11 ’ ’i 1' ■111 . ■ । । ‘A H- .k K . । ' । । । > i i । i । i i । i i । I ] । i i r । f < i i | I I I I [ I I I I | I I I I | I r ITIT

m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 41.20 41.40 41.60 41.80 42.00

0402LB.D SCAN020403.M Thu Apr 04 10:14:26 2002 Page 9

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