GCMS results for sample AE08068, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08068.D vial : 25 Acq On : 16 Apr 2002 6:25 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 1 2-Butene, l-chloro-2-methyl- Concentration Rank 20

R.T. EstConc Area Relative to ISTD R.T.

4.06 0.33 ug/L 219072 1,4-Dichlorobenzene-d4 9.99 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butene, 1-chloro-2-methyl- 104 C5H9C1 013417-43-1 14 2 2-Heptyne, 7-chloro- 130 C7H11C1 070396-13-3 10 3 1-Butene, 2 -(chloromethyl)- 104 C5H9C1 023010-02-8 9 4 2-Butene, l-chloro-3-methyl- 104 C5H9C1 000503-60-6 9 Abundance Scan 167 (4 060 min) 08068 D (-159) (-) m/z 43.30 100.00% 48

5000 69 57 ■ 1 1 ■ 1i"u ■ । i ■ ■ ■ >• । ore . । . . . 51 77 88 104 120 3.80 4.00 4 20 4 40 0+ 1 * ' ■ I hl | h -...... 4 m/z 41.30 53.22% n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2493 2-Butene, 1-chloro-2-methyl- 41 69

5000 53 104 3.80 ' 4 00 ' 4.20 ' 4.40 27 m/z 69.30 31.97% 89 0- । 36 >li I ), . li), । 201 63 1751,...... J........ I 1 1 1 1 i 1 ■ 1 1 I ' 1 1 1 i 1 1 ■ i ' 1 ■ ' i 1 T’I n/z-> 20 3p 40 50 60 70 80 90 100 110 120 Abundance #2812 2-Heptyne, 7-chloro- 41 88 81 3.80 4.00 4.20 4 40 27 54 5000 m/z 39.30 20.97% 67

.. .. 1361 +ll 49 62 75 , 101106 115 01 -44—4 4—— n/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #2524: 1-Butene, 2-(chloromethyl)- 41 60 1***WI’’II’II’IFTI’’’ 3.80 4 00 4 20 4 40 m/z 57.30 16.49% 55 5000- 27 104

n/z-> 0 I ■. iMn --lill 20 30 36

40 +l 50 49 60 63 t-, 111 70 4.80—ed 90 75 ...... 100 89 1 M.,110" ■ । । * ■ > ■ । 120 ... in..... 3.80 4.00 4.20 4.40

08068.D 041202SCAN.M Tue Apr 16 13:56:50 2002 Page 4

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