GCMS analysis results for sample AE08063, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \MSDCHEM\1\DATA\020415\08063 .D Vial: 20 Acq On 16 Apr 2002 2:21 am Operator: Nefliu Sample sample Inst : Instrumen Misc Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C: \MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 Acetonitrile, dichloro- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

3.67 0.37 ug/L 315636 1,4-Dichlorobenzene-d4 9.99

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

U 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Allyl mercaptan 74 C3H6S 000870-23-5 25 3 Thiirane, methyl- 74 C3H6S 001072-43-1 5 4 IH-Pyrazole, 3-methyl-____________ 82 C4H6N2 001453-58-3 5 Abundance Scan 100 (3.667 min) 08063 D (-95) (-) m/z 74.20 100.00% 74

82 5000 47 38 3.40 360 3 80 4 00 0+ - • i • 1 < < i 1 i , "bi . 88.. ..... m/z 82.20 51.18% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338' Acetonitrile, dichloro- 74

5000 82 .N h 47 3.40 3 60 3 80 4.00 m/z ;76.20' 32.26% 35 12 26 — . . 62 ! .1 ■ i • • ■ ■ ■ I > > 108 0+ 1 ’ 1 1 TT+ ■ ■ i 1 ■ ' 1 i 1 1 i-| 1 ' 1 > I

n/z-> 10 20 :30 40 50 60 70 80 90 100 110 Abundance #28161 Allyl mercaptan 4n 74

3.40 3.60 3 80 4.00 5000 m/z 84.20 30.09%

47 nkununou n/z—> 0+ -l ,1,,52.52...89,0 10 20 27 33 30 1 40 50 60 70 80 1 1 i ' 1 ■ ' i ■ ■ ■ ' I"1 1 1 ' 1 1 1 1 1 I 90 100 110 Abundance #115343 Thirane, methyl- 41 74 3.40 3 60 3.80 4.00 m/z 47.20 25.52% __ 5000

47 27 „ 0 ................ . + »11’, ’,l 154' "*i59 6469, ' । । II ‘ I . । . . . ■ ( . । . ■ . . । ■ ■ ' ' । /z—> 10 20 30 40 50 60 70 80 90 100 110 3 40 3 60 3.80 4 00

08063 .D 041202SCAN.M Tue Apr 16 13:51:55 2002 Page 6

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