GCMS analysis results for sample AE09156, May 2002

NYC 9/11 Public Portal Document

• Data File : C:\MSDCHEM\1\DATA\020424\09153.D Vial : 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title Method 508 GC/MS Scan Library C:\DATABASE\nist98.1 Peak Number 2 Acetonitrile, dichloro- Concentration Rank. 6

R.T. EstConc Area Relative to ISTD R.T. 3.65 0.25 ug/1 313624 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 32 3 Furan, 2-methyl- 82 C5H60 000534-22-5 9 4 Allyl mercaptan 74 C3H6S 000870-23-5 5 Abundance Scan 97 (3.649 min): 09153.D (-93) (-) m/z 74.10 100.00% 74

82 5000 40 47 p-r F . .............. ■ ‘ । 1 3.40 3.60 3.80 4.00

/z—> 1 ' i ■ 1 ' ■ I 1 ' . ' I ' 10 20 30 ll 40 50 60 _________ L 44484, ■ i ■ . < • i ■ 70 80 90 100 110 m/ z 82.00 51.62% Abundance #28338: Acetonitrile, dichloro- 74

5000 82 *, #,4 , . 3.40 3.60 9 3.80 4.00 47 m/z RWv—RA~WwAl 40.10 42.43% 35

n/z-> I 10 12 26 1 i 1 1*ti । 1 '.1 । । 20 30 I Jl 40 ll.... 50 60 2.111 70 , 108 TI3 I"IIItIIIIIEIIIi 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 3.40 3.60 3.80 4.00 5000 82 m/z 76.10 35.80% 47

■i-,-i । । । i-i-i । । । i'i TI1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #32366: Furan, 2-methyl- _A 82 3.40 3.60 3.80 4.00 m/z 84.00 27.76% 5000

15 27 39 53

w*shyup/ypusL m/z- > rr"I ' i'' । । । 10 T I * I I * | 1 1 , llpeal, I 20I 30 40 50 60 Ji 70 ...80JI 90 100 110 TI 3.40 3.60 3.80 4.00

09153.D SCAN020424.M Fri May 03 11:00:23 2002 Page 4

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