GCMS analysis results for sample AE09156, May 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\DATA\020424\09153.D Vial: 22 Acq On : 25 Apr 2002 6:29 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020424.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Chloroform Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T.

3.35 0.21 ug/1 273078 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

-1—Chloroform 118 CHC13 000067-66-3 86 2 Methane, bromodichloro- 162 CHBrC12 000075-27-4 83 3 Chloroform 118 CHC13 000067-66-3 78 4 Methane, oxybis[dichloro- 182 C2H2C140 020524-86-1 78 Abundance Scan 46 (3.349 min): 09153.D (-38) (-) m/z 83.00 100.00% 83

5000 40

m/z-> Abundance ■' । ■ ■ ■ ■ । 10 20 ■111' 30 + 40 50 — "I i ■' " i'' " i 60 70 80 90 100 110 120 130 140 150 160 170 #116499: Chloroform 129 11 ’ 1’ i' " ' i ,1, Mrm" MTMn MAh 111 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/ z 85.00 69.36%

83

5000 A M4, A A TMY N MAMA M4M*Y 3.20 3.30 3.40 3.50 3.60 3.70 3.80 47 m/ z 40.10 47.81% 35 — | 118 P TTTT'' ।" " ।" " ।" il11111"111TT i1"1111’111" m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #33236: Methane, bromodichloro- 83

3.20 3.30 3.40 3.50 3.60 3.70 3.80

w 5000 m/z 47.10 20.24%

47 129 13 27 ' i ■' ■ ■ i1 TTTT 10 20 30 25. 60 70 80 13 40 63 72 N| ■ i1 ■ ■ ■ i ■1 ■ 'i111 ■ । > । ■ ■ ।

90 100 110 120 130 140 150 160 170 50 116 ||, ..... I'11111'11 r ''11'' 164 111'' " i ‘1'' i111 1 Vh Abundance #33238: Chloroform i' ■'' i1'1 ■ ir 1' ■ i1' ■ ■ i l""i" 80 3.20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 128.90 14.20% 5000 47

TIIU"UTIT 27 $0,797# ..................... 96 118 It i1 " ' i " " r 1 " i T’T i'1 ‘ ‘ i " ■ ■ i''r ■ i " ■n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 3.20 3.30 3.40 3.50 3.60 3.70 3.80

09153.D SCAN020424 .M Fri May 03 11:00:21 2002 Page 3

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