GCMS reference results for sample AE10772, May 2002

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Gas chromatography-mass spectrometry reference report for sample AE10772 listing measured values and detection limits.

NYC-WTC_000045849–000045858

Folder label: “GCMS X 5/6/02 A 5/11/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAY1002\10772.D Vial: 16 Acq On : 11 May 2002 3:41 am Operator: Sample : GC/MS SCAN 5/6 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.76 0.53 ug/1 55238 Naphthalene-d8 15.80

Hit# 5 Tentative ID MW MolForm CAS# Qual 1 clopentasiloxane , decamethyl- 370 C10H3005Si5 000541-02-6 83 enzeneethanamine, FT7 [ (penlafluorop 563 C24H34F5NO3Si3 055429-13-5 38 3/N-(Trifluoracetyl)-0,0',O"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 28 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 28 Abundance Scan 1061 (14.765 min): 10772.D (-) m/z 73.10 100.00% 73 A 5000 267 355 T7 45 14.40 14.60 14.80 15.00 15.20 J 1 I | I I I ! 154 191 223 TTTdT ] l1 I I F j 1 T*-1 ! J 1 I I ] I I I 1 7 I I I [ I I I I | I r rI -j T ‘r* r-1" ‘‘"T m/z 267.05 31.49% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 TF 1T 17 14.40 14.60 14.80 15.00 15.20 m/z 355.10 25.66% 323, | ......... 207 m/z—>___ 50 — 100 150 200 H-300 250 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 / TT TT TT 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 9.29%

45 208 251 281 386 458 548 ' 1 i 1 ' i l l r i ■ । i i i r । i i i i | । । r" i " | "r I i i । ~ i ii । । । । i । 1 r-1 IIIIII r m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(Trifluoracetyl)-O,O',O"-tris(trimethylsilyl)epin £ 73 TT Tr 14.40 14.60 14.80 15.00 15.20 355 m/ z 74.10 8.32%| 5000

45 I 140 184 281 480 ........ II.......... — m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

10772.D GCMS0510.M Mon May 13 14:18:22 2002 Page 2

NYC-WTC_000045857

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