GCMS calibration table for sample AE09447, May 2002

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Technical document displaying GCMS calibration data and compound retention times for sample AE09447 processed in early May 2002.

NYC-WTC_000045472–000045479

Folder label: “GCMS X 5/3/02 A 5/8/02”

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Data File C:\HPCHEM\1\DATA\MAY0202\9447.D Vial: 6 Acq On 2 May 2002 7:41 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Pentane, 3-methoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.10 0.64 ug/1 53426 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 3-methoxy- 102 C6H140 036839-67-5 23 2 1,3-DioxolAne, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 2,21-Trimethylenebis-1,3-dioxolane 188 C9H1604 006543-04-0 9 Abundance / Scan 333 (8.095 min): 9447.D (-) m/ z 73.10 100.00% 73

5000 43 i i r । i i ।_ । । ii । । । । ii i । । i । ।

7.80 8.00 8.20 8.40 36 ul, ,| 49 55 । | । 87 103 ' 1 i 1 1 1 ’ i ' 1 I ' ' ' ' 1 1 1 1 1 I 11 1 1 I I TTT TTTTTTTETTT m/z 43.05 31.44% m/z-> 10 20 30 40 50 70 80 60 90 100 110 120 Abundance #1793: Pentane, 3-methoxy- 7)3

5000 । । । । । । । । । । । r i । ki i r । > ■ i t 45 7.80 8.00 8.20 8.40 m/z 41.10 11.39%

miz-> 10 20 47,33.3%30 40 ' 1 1 50 55 ).......... I'1 60 70 80 90 100 110 120 Abundance #49423:1,3-Dioxolane, 2-(3-bromo-5,5,5-trich!oro-2,2-dimet 73 '1111■11i1111i''11i''rr 7.80 8.00 8.20 8.40 5000 m/z 45.05 11.29% 45

................ 361| I r I I I I I I I I I I I I I I I I I I I * I I 55 67. >1 । । r "। ~r । । । — । । । । i । [ । । । FT 109115 m/z-> Abundance 10 20 30 40 50 60 70 80 #62932: Silane, tetramethyl- 73 90 100 110 120 My... I । ।

7.80 | 11 1 1

8.00 | 11 1 1

8.20 | ' । A.... 11

8.40 | 1 : । ।

m/z 71.10 7.10%

5000

45 15 , 53 59 I-TI I 88 , 1 i i ( । i i i | I । I । j i i i । । i r

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

9447 .D GCMS0501.M Fri May 03 08:40:52 2002 Page 1

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GCMS calibration table for sample AE09448, May 2002 · Box DEP Box 25

NYC-WTC_000045490

Technical document displaying GCMS calibration data and compound retention times for sample AE09448 processed in early May 2002.

1 shared topics · Same agency, volume and box · similarity 0.999