Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10304 conducted on May 17, 2002.
NYC-WTC_000045092–000045112Folder label: “GCMS X 5/1/02 A 5/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\MSDCHEM\1\DATA\050802\10304 .D Vial: 7 Acq On 8 May 2002 6:41 pm Operator: Mclean Sample 5/1 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chernstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 6 1,3,5-Triazine-2,4,6(1H,3H,... Concentration Rank 8
R.T. EstConc Area Relative to ISTD R.T.
5.06 0.30 ug/L 202916 1,4-Dichlorobenzene-d4 9.93
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,3,5-Triazine-2,4,6(1H,3H,5H)-t... 129 C3H3N303 000108-80-5 5 2 2-Chloro-4-aminopyrimidine 129 C4H4C1N3 007461-50-9 5 3 Imidazole, 4-fluoro-5-aminocarbo... 129 C4H4FN3O 033300-35-5 4 4 1,3,5-Triazine-2,4,6(1H,3H,5H)-t... 129 C3H3N303 000108-80-5 4 Abundance Scan 338 (5.065 min): 10304.D (-335) (-) m/z 128.90 100.00%| 129
5000 47 79 91
m/z-> 0........ . 20 30 44 40 50 58 1 1 I 1 1 1 1 I 1 1 1 ‘ i ' ■■■i1‘11i ■ 1 ' 1 i 1 ‘ 1 ' 1 1 1 11 I 1111।1 1 1 1 । 1 * 60 70 80 90 100 110 120 130 140 150 4.80 m/z 130.90 5.00 5.20 5.40 40.85% Abundance #121801:1,3,5-Triazine-2,4,6(1 H,3H,5H)-trione 129
44 5000 171’1’’’11111+++II1 4.80 5.00 5.20 5.40 86 m/z 47.00 34.64% 70
miz-> Abundance 0- ■ > । 20 29 ‘ ■ i11 ■ • * । ।' l 30 40 — 54,. 50 60 70 80 90 100 110 120 130 140 150 #58331:2-Chloro-4-aminopyrimidine "MMMMMywMMM 119
94 4.80 5.00 5.20 5.40 5000 m/ z 43.10 33.21% 28
35,iI1 O—T '|, i"i 41
i +ll—1.59+4— 52 1+ ils TT 111 0 77 86 67
116 102 MwMhws/ m/z-> 20 30 40 50 60 70 80 90 100 110 I 120 130 140 150 Abundance #58386: Imidazole, 4-fluoro-5-aminocarbonyl- 1 ‘ 1 ' 1 1 1 1 1 I 1 1 1 1 1 1 1 '' 1 1 1 1 1 129 4.80 5.00 5.20 5.40 m/z 49.90 33.04%
5000 113
44 58 85 I 51 ,h 67 74 i 100 | 0 ' ' I ' ' ' ' I ' ' ' ' I'1'1'1 1 I I'1 ’I । | ■ । । ' l I' । ' । I I | I 1'1 I | I I I । | ! I 1-1 |’l I ! | I I । 145 'I 1 ''1 i1 1 I T m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 4.80 5.00 5.20 5.40
10304.D 050102.M Thu May 09 13:50:23 2002 Page 9
NYC-WTC_000045105
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NYC-WTC_000045137
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10306 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045075
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10303 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044071
Laboratory report for sample AE09971 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043938
Gas chromatography-mass spectrometry analysis report for sample AE09968, detecting unknown compounds and 2,4-DDD surrogate with 78% recovery, dated May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043976
Laboratory report for sample AE09970 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045171
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10308 conducted on May 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044025
Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044885
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000044994
Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10204 on May 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022763
GCMS analytical report for environmental sample AE09331 including surrogate compound data from May 15, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012989
Laboratory report presenting analytical results for target compounds and surrogate recovery data for water sample AE11907.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024014
Laboratory report showing GC/MS analysis of sample AE10985 with surrogate recovery data for 2,4-DDD.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000045045
Department of Environmental Protection GCMS analysis record for the World Trade Center site dated May 1-8 2002.
Filed in the same folder
NYC-WTC_000045046
Administrative page listing laboratory method details, sample volumes, and surrogate addition parameters for environmental testing on May 2002.
Filed in the same folder
NYC-WTC_000045048
Laboratory report showing blank analysis results for volatile organic compounds in sample AE10303 on May 9, 2002.
Filed in the same folder
NYC-WTC_000045063
Laboratory report detailing quantitative analysis of volatile organic compounds in environmental sample AE10303 conducted on May 9, 2002.
Filed in the same folder
NYC-WTC_000045067
Laboratory record containing manual entry reference values for volatile organic compounds in environmental sample AE10303 from May 9, 2002.
Filed in the same folder