GCMS surrogate recovery report, sample AE12763, June 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\061102\12763.D Vial: 7 Acq On : 11 Jun 2002 2:46 pm Operator: Sample : re-ext. Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 2-Chloro-4-aminopyrimidine Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 5.02 0.41 ug/L 335342 1,4-dichlorobenzene-d4 9.90 Hit# of Tentative ID MW MolForm CAS# Qual 1 2-Chi o-4-aminopyrimidine 129 C4H4C1N3 007461-50-9 5 2_ _5-F1 -roimidazole-4-carboxylic a... 129 C4H4FN30 1000129-62-3 4 3 3-Thio-1,2,4-triazin-3,5(2H,4H)-... 129 C3H3N30S 1000213-20-1 4 4 Goitrin 129 C5H7N0S 000500-12-9 2

"Mo Abundance Scan 330 (5.018 min): 12763.D (-326) (-) m/z 47.00 100.00% 47 129

5000 38 87 4.60 4.80 5.00 5.20 5.40 0 » * 1 * 1 1 • I « ' I1 ■ ■ i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ ■ ■ ■ |1’1’’I1**11**’’I+* ■ ■ । ■ ■ ■ ■ । m/z 128.80 75.33% niz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #58331:2-Chloro-4-aminopyrimidine 12.9

5000 67 94 . ...... Mk 4.60 4.80 5.00 5.20 5.40 41 102 28 m/z 126.90 64.97% , 52

mz-> O—T 20 ++ 3511111,-177159... 11*1 t 77’i* ■ 186Ptl 30 40 50 60 70 80 90 100 110 116 +tT r 120 130 Abundance #58224:5-Fluoroimidazole-4-carboxylic amide

44 113 129 ..... M..... 4.60 4.80 5.00 m/z 48.00 5.20 5.40 44.74% 5000 58 85

0-PP —ll++ /67...TmmgT —ll—PPP m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #58194:3-Thio-1,2,4-triazin-3,5(2H,4H)-dione 42 1:9 4.60 4.80 5.00 5.20 5.40 m/z 38.10 40.30% 5000 60 Ml W My A A 71

m/z—> 0-mmm 20 30 40 1149,. 50 I 1 60 86 95 101 113 III 78 +119 70 80 90 — IP 100 110 120 130 4.60 4.80 5.00 5.20 5.40

12763.D 060302.M Tue Jun 11 15:54:11 2002 Page 16

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