GCMS analysis results for sample AE06339, May 3 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050102\6339.D vial: 15 Acq On 1 May 2002 9:06 pm Operator: Mclean Sample re-ext 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified’ GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 5-Fluoroimidazole-4-carboxy... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

5.12 0.20 ug/L 146845 1,4-Dichlorobenzene-d4 9.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 5-Fluoroimidazole-4-carboxylic a... 129 C4H4FN30 1000129-62-3 9 2 dl-lsocitric acid lactone 174 C6H606 004702-32-3/9 3 1,3,5-Triazine-2,4,6(1H,3H,5H) -t... 129 C3H3N303 000108-80-5 7 4 1,3,5-Triazine-2,4,6 (1H,3H,5H)-t... 129 C3H3N303 000108-80-5 7 Abundance Scan 347 (5.118 min): 6339.D (-341) (-) m/z 128.88 100.00% 129

44 56 5000 ______________ 35 72 81 I I I I I I I I I I I'I I t I I I I I 1 1 I _................. I... I I I I 1 I I I I I I I I I I I I I I I I I I IIII I I I I I I 4.80 m/z 126.90 5.00 5.20 5.40 70.74% m/z-> 10 20 30 40 50 7060 80 90 100 110 120 130 Abundance #58224: 5-Fluoroimidazole-4-carboxylic amide 129

44 113 5000 1 1 ■ i ■ 1 1 1 I 1 1 ' 1 i 1 1 1 ' i 1 ‘ 1 ■ I

58 4.80 5.00 5.20 5.40 85 m/z 44.10 61.60%

Ti/Z—> Abundance 1 1 । 1 1 .................. 10 20 30 40 50 TIt 1 1 1 ' ' ' I ' 1 1 1 I

#121803: dl-lsocitric acid lactone 55 11....... 60 70 80 ' I 1 1 ' 1 I ' ' ' 1 1 1 1 1 1 i 1 1 ' ' I ■ 90 100 110 120 130

129 TTF Apokouosr 101 1 1 ■ i ■ ‘ I I I I I I I I I I I I I I I I I I

4.80 5.00 5.20 5.40 84 5000 27 m/ z 56.10 60.69% 39 45 73 91 111 1+ ! | 6511, r . — - 121 1 I 1 1 1 1 I /z-> Abundance ■ ■ ■ । ■r

10 20 30 40 50 60 70 80 #58201: 1,3,5-Triazine-2,4,6(1 H,3H,5H)-trione 90 100 110 120 130

129 .. II... 4.80 5.00 5.20 5.40 m/z 57.10 42.86% 43 5000

70 86

m/z-> 15 ■ ■ i 1 ' ■ 1 i ‘ 10 20 44.38,1 50 60 70 80 90. 100 110112 120 30 40 54......................... ' I1 1 ' I ' 1 ■ ■ I 130 1 ' i ' 1 ■ ■ i ' 1 1 1 I ■ 1 1 4.80 5.00 5.20 1 i 1 1 ' 1 i 5.40

6339.D 050102.M Thu May 02 12:24:27 2002 Page 6

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