GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 18 Molybdenum, tetrakis(.eta.3-2- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

43.01 0.63 ug/1 69255 Perylene-dl2 37.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Molybdenum, tetrakis(.eta.3-2-prope 360 C12H20Mo2 012318-77-3 12 2 1H-Indene, l-ethylideneoctahydro-7a 164 C12H20 056362-87-9 10 3 Benzaldehyde, O-ethyloxime 149 C9H11NO 013858-87-2 9 4 Furo [2,3 -c]pyridine, 2,3-dihydro-2, 149 C 9H11NO 069022-82-8 9 Abundance Scan 4136 (43.013 min): 8757.D (-) m/ z 55.00 100.00% 55 93 2 5 149 233 5000 1121 401 „Mwv I ! 177 253 281 383 V I ' 1 42.60 42.80 43.00 43.20 43.40 J m/z 93.00 95.67% TT TT i1'" i' " i"1 j |l+ i i । । । *1 । Tri । । । । 11 । ii । < | ri r> । । i i । । । । । । । 11 । । I mlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #50290: Molybdenum, tetrakis(.eta.3-2-propenyl)di- 2 5

5000 175 i 1 ' 1 1 i • 1 42.60 42.80 43.00 43.20 43.40 m/z 215.15 95.29% । । । । । । । । . । । । । । ri । '| rri । । । । । । । । i . । । । । ^” । .'1 262 I I I < I I I i i । i i n~j r>"rr II II I I I I I I I 11'1I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #13591:1 H-Indene, 1 -ethylideneoctahydro-7a-methyl-, cis- 149 93 i 1 1 1 1 i 1 ' 42.60 42.80 43.00 43.20 43.40 67 121 m/z 149.00 80.79% 5000

| " 1 1 t 1 1 1 ' |T> " | ii । | | | I. I.. I. I. ‘T’’’’ I >... I.... 1.1111... 11.. 1111111 [ 1111111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #9482: Benzaldehyde, O-ethyloxime 149 42.60 42.80 43.00 43.20 43.40 m/z 69.00 74.76% 77 A 5000 104 51 121

I 1 ,1 i ■1 ’1 r " 11'1" i'111 r ■ ‘‘E‛TTrI‛17 > ।. 1111, । -1 p ,, 11111111111 [ 11111 i'1" i 111" ’ ■ i " 1 ' i 1 b m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320340 360 380 400 42.60 42.80 43.00 43.20 43.40

8757.D GCMS0412.M Tue Apr 23 08:23:11 2002 Page 18

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