GCMS chromatogram data for sample AE04592, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2602\4592.D Vial: 8 Acq On 26 Mar 2002 4:38 pm Operator: Sample gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 8 3,6-Dioxa-2,4,5,7-tetrasilaoct Concentration Rank 8.

R.T. EstConc Area Relative to ISTD R.T.

45.53 0.82 ug/1 68160 Perylene-dl2 37.94

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-Dioxa-2,4,5,7-te1^asilaoctane, 294 C10H3002Si4 004342-25-0 35 2 1-Monolinoleoylglyc^ol trimethyl'si 498 C27H54O4Si2 054284-45-6 17 3 Ergotaman-3',6',IS-Zrione, 12'-hydr 561 C31H39N5O5 000564-36-3 10 4 Benzophenone-2,4',7-tricarboxylic a 356 C19H16O7 000000-00-0 . 9 Abundance Scan 4410 (45.534 min): 4592.D (-) m/ z 43 ■ 147 221 5000 281 355 429 ' r ' r, . I . . [

..... -14 50 I 96 100 150 200 177 L 250 , 300 350 400 Tl i I 450 45.20 45.40 45.60 45.80 m/z 147.00 65.89% Abundance #41682: 3,6-Diox3-2,4.5,7-tetrasilaoctane, 2,2,4,4,5,5,77- 147 221

73 AAA 5000 45.20 45.40 45.60 45.80 191 117 279 m/z ■221* 05 55.75% t.... ..... .. m/z-> _ 50 100 150 200 250 300 350 400 450 Abundance #588<1: l-i'.'tonoli'ialeo/glycer&i t.-imethylsilyl ether 73 I ' ' ' ' I ' ' ' 'I ' ' ' ' I 207 ___ 45.20 45.40 45.60 45.80 5000 147 m/z 207.00 37.72% 34 103 281 I,.................... '......................... ' , , ......................... 482 m/z-> 50 100 150 200 250 300 350 400 450 Abundance- #60299: Ergotaman-3',6',18-trione. 12'-hydroxy-2',5'-bis(1- 413 __457g^_45A^_4Jti0 45jp_____ 70 m/z 355.05 ' * 28 .'93%

I 5000

IN I 50 98

100 154

150 I 195 I 221 ll I I 200 250 267

294 300 346 350 400 450 _, I. a/ 45.20 45.40 45.60 45.80 a a _

4592.D GCMS0308.M Thu Mar 28 16:28:27 2002 Page 8

NYC-WTC_000058405