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GCMS chromatogram data for sample AE04593, April 2002

Machine-extracted title · confidence 100%

Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04593.

NYC-WTC_000058407–000058415

Folder label: “GCMS X 3/4/02 A 3/26/02

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Scanned page image, NYC-WTC_000058414
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR26O2\4593. D Vial: 9 Acq On : 26 Mar 2002 5:38 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 ’ Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1,

R.T. EstConc Area Relative to ISTD R.T.

8.14 1.90 ug/1 309146 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, ^tramethyl- 88 C4H12Si 000075-76-3 37 2 1,3-Dio3^1ane, 2-methyl- 88 C4H8O2 000497-26-7 9 3 N-EthyPformamide 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 9 'Abundance Scan 337 (8.137 min); 4593.b”{-) m/z 73.0^^100.00% /la

5000 43 ' I ' ' ‘ ' I 87 103 7.80 8.00 8.20 8.40 __ ' 0 ‘ .............. 3? I, I 50 5/ ■ ■ 67, I m/ z 43.05 27.12% m/z->^10 20 30 40 50 I60 70 80 90 100 110 Abundance #845; Silane, teframethyi- 7)3

5000 - I - 7-80 8.00 8.20 8.40____ 45 m/z 41.05 io“68% ^1® 31 . .1 55 I 88 m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62002: 1.3-Uioxoiarie. 2-rnetbyi- 73

7.80. 8.00 8.20 8.40_____ 5000 43 m/z 45.05 10.52% 58 27. 87

m/2--> 10 20 30 40____ 50____ 60____ 70____ 80____ 90____100___ 110 Abundance #292: N-E(hylformamide 33 7.80 8.00 8.20 8.40 73 m/ z 71.00 7.39%

m/z-> 5000

10 15 20 4 30 40 44

50 58

60 70 80 100 110 7.80 8.00 L 8.20 8.40

4593.D GCMS0308.M Thu Mar 28 16:29:14 2002 .Page 1

NYC-WTC_000058414

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NYC-WTC_000058414Source: NYC Law Department, mirrored locally

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