GCMS analysis results for sample AE04731, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR26O2\4731.D Vial: 13 Acq On : 26 Mar 2002 9:35 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 1.90 ug/1 297157 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Silane, t^tramethyl- 88 C4H12Si 000075-76-3 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 3-PentaK(ol, 3-methyl- 102 C6H14O 000077-74-7 9 4 Pentan^, 3-methoxy­ 102 C6H14O 036839-67-5 9 Abundance ■ ..... ...... ................... Scan 3367i^134 min)?473l'D (-)' m'/z.... 73?^.... iooT^ : 7b

5000 43

I 55 87 .103 7.80 8.00 8.20 67, I m/z 43.05 29.37% m/z-> 10 20 30 40 50 60 70 80 90 100 110 ■Abundance #62932: Silane, tetramethyl- 7^

5000 7.80 8^00 8.20 45 m/z 11.56%

L 15 ............................... r , , 53 59 88 I ' ‘ ' I m/z->______ 10 20 30 40 50 60 70 80 90 100 110 Abundance rf'&'Z: N-1my■ ’crrnamide 30 73 I ' I 7.80 8.00 8.20 8.40 5000 m/ z 45.05 10.12% 58 i 15 __ 10 20 30 40 50 .60 70 80 90 100 110 ’Abundance #63572: 3-Pentanoi, 3-methyi- 713 7.80 8.00 8.20 8.40 m/ z 71.00 7.04% 5000 55 45 87 I 27 I i 'I" I J................ 10 20 :30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

4731.D GCMS0308.M Thu Mar 28 16:32:39 2002 Page 1

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