GCMS analysis results for sample AE04732, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\4732.D Vial: 14 Acq On : 26 Mar 2002 10:35 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Silane, tetramethyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.14 1.81 ug/1 275328 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual A--------------------- 1 Silane (tramethyl - 88 C4H12Si 000075-.76-3 25 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dic^olane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 2-methyl- 88 G4H8O2. 000497-26-7 4 Abundance ScS 337 (SJ 37 min): 473fD'(-) m/z 737d0 100.00% 7)3

5000 43

87 103 7.80 8.00 8.20 8.40 , m',-| 67, I I " I ' I ' m/ Z 4 3.00 29.20% ni/z-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #62932: Silane, tetramethyl- 713

5000 __ 7^__ 8.00 8.20 8.40____ 45 m/ Z 41.05' 10.63% 15 53 59 88 ! f-rY-r^T-ryT-r-T-r-i-TT-rT-r^-^ m/z->10 20 30 40 50 60 70 80 90 100 110 120 Abundance ' N-Etnylformarnide 30 73 ' ' I ' ' ' ' I 7.80 8.00 8.20 8.40 1 5000 m/ z 45.05 10.42% I 44 58

15. ............... I j ,......... ........... ............................................ ___ 10 20 30___ 40___ 50 60____ 70___ 80____90___ 100__ 110___ 120 Abundance #4942i 1,3-Dioxolane, 2-(3-bromo-5,5,5-trichioro-2,2-dimet ...................... 713 7.80 8.00 8.20 8.40 m/z 71.00 7.44% 5000

45 36 ,|| 55 ^■^1 ................................. 1,09115 I , 10 20 30 40 50 60 70 80 90 100 110 120 7.80 8.00 8.20 8.40

4732.D GCMS0308.M Thu Mar 28 16:33:14 2002 Page 1

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