GCMS calibration table, May 2002

NYC 9/11 Public Portal Document

Data File C : \HPCHEM\ 1 \DATA\MAYO 102\9398.D Vial: 16 Acq On 1 May 2002 9:54 pm Operator: Sample gc/ms scan 4/18 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butane, 2-methoxy-2-methyl- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

8.11 0.57 ug/1 35052 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane/ 2-methoxy-2-methyl- 102 C6H140 000994-05-8 36 2 Propane, 2-methoxy-2-methyl- 88 C5H120 001634-04-4 9 3 1-Octanamine 129 C8H19N 000111-86-4 9 4 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 Abundance Scan 335 (8.108 min): 9398.D (-) m/z 73.10 100.00% 73

5000 43

1 , 55 87 7.80 8.00 8.20 8.40 ■ ' i ■ ■ ‘ ■ i ' ... ..................... 'I1' f r ■ i ■ 1 1' ■ i ■ ■ ■ ■ । ■ ■ ■ ■ i ■ • > ■ i ■ ■ > ■ i ■ m/z 43.05 37.68% mlz->_____ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63526: Butane, 2-methoxy-2-methyl- 73

5000 _ - | — 55 7.80 8.00 8.20 8.40 87 m/z 41.15 15.26% 27 45

m/z-> 10 20 30 40 50 —P P 1 I I I I I I I I I I I I I I I I I I I I I > I > I I I I I I

60 70 80 90 100 110 120 130 Abundance #862: Propane, 2-methoxy-2-methyl- 73

7.80 8.00 8.20 8.40 5000 m/z 45.05 12.34% 29 41 57 15

TP—H—PPPPP m/z-> Abundance 10 20 30 40 50 60 70 #65171:1-Octanamine 80 90 100 110 120 130 Mow _ A /......M ‘‘‘ i 11 ' ' i ‘ 1 ■ 1 i 1 1 1 1 i " 1 1 i 33 7.80 8.00 8.20 8.40 m/z 39.10 9.11%

5000

41 I , 55 69 86 129 1 11 I I I '" I I-1 I I I I I I 11 1 1“ I I I I I I I I I I I I I I I I I I I ————— T 1 1 11 T f" I l" ( I I I I I I I " 11 1 T m/z~> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40

9398.D GCMS0501.M Thu May 02 12:04:35 2002 Page 1

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