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GCMS analysis results, sample AE09393, May 8, 2002

Machine-extracted title · confidence 95%

Laboratory report for DEP Box 25 showing GCMS analysis of sample AE09393 with unknown compounds and surrogate data from May 8, 2002.

NYC-WTC_000043079–000043096

Folder label: “GCMS X 4/18/02 A 5/1/02

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NYC 9/11 Public Portal Document

Data File C:\HPCHEM\1\DATA\MAY0102\9393.D Vial: 11 _ Acq On 1 May 2002 5:16 pm Operator: Sample gc/ms scan 4/18 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.110 330 335 339 rBV 17236 39868 1.00% 0.185% 2 8.175 339 342 373 rVB 426539 1011750 25.48% 4.705% 3 12.207 776 782 799 rBV 1290653 2900692 73.05% 13.489% 4 14.809 1061 1066 1071 rVB 47395 93730 2.36% 0.436% 5 15.835 1172 1178 1195 rBV 1724711 3687317 92.86% 17.147%

6 17.961 1406 1410 1415 rVB 61994 116886 2.94% 0.544% 7 18.676 1483 1488 1493 rBV 23848 42537 1.07% 0.198% 8 20.793 1714 1719 1724 rBV 48257 92013 2.32% 0.428% 9 21.141 1751 1757 1767 rBV 1955421 3970843 100.00% 18.466% 10 21.563 1796 1803 1808 rBV 19806 39924 1.01% 0.186%

11 23.276 1983 1990 1999 rBV2 181233 431424 10.86% 2.006% 12 25.485 2225 2231 2235 rBV 27407 56169 1.41% 0.261% 13 25.585 2235 2242 2253 rW2 1762218 3786643 95.36% 17.609% 14 25.723 2253 2257 2264 rVB 17562 41379 1.04% 0.192% 15 27.418 2435 2442 2447 rVB 20417 41069 1.03% 0.191%

16 33.640 3112 3121 3137 rBV2 1312344 2943656 74.13% 13.689% 17 33.860 3140 3145 3154 rVB 28113 70950 1.79% 0.330% 18 37.874 3574 3583 3596 rBV2 742597 2136760 53.81% 9.937%

Sum of corrected areas: 21503610

9393.D GCMS0501.M Thu May 02 12:02:37 2002

NYC-WTC_000043084

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NYC-WTC_000043084Source: NYC Law Department, mirrored locally

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GCMS calibration table, May 2002 · Box DEP Box 25

NYC-WTC_000043146

Laboratory document displaying a GCMS calibration table with retention times and response factors for deuterated standards from May 2002.

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