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GCMS unknowns report for sample AE02561, March 2002

Machine-extracted title · confidence 90%

Laboratory report detailing analysis of unknown compounds and surrogate recovery for sample AE02561.

NYC-WTC_000038784–000038800

Folder label: “GCMS X 3/4/02 A 3/20/02

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Scanned page image, NYC-WTC_000038789
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NYC 9/11 Public Portal Document

Data File : C:\HPCHEM\l\DATA\MAR1902\2561.D Vial: 20 Acq On : 20 Mar 2002 11:43 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.146 334 338 349 rBV 32919 72815 1.84% 0.358% 2 12.268 782 787 802 rVB 1210459 2717017 68.67% 13.347% 3 14.866 1064 1070 1076 rVB 119966 238191 6.02% 1.170% 4 15.904 1177 1183 1200 rBV 1793849 3624460 91.61% 17.805% 5 18.024 1408 1414 1419 rVB 48277 95253 2.41% 0.468%

6 18.741 1487 1492 1496 rBV 41756 76132 1.92% 0.374% 7 20.861 1718 1723 1728 rVB 34702 67328 1.70% 0.331% 8 21.210 1755 1761 1774 rBV 1830062 3956531 100.00% 19.436% 9 23.386 1991 1998 2003 rBV 25864 49856 1.26% 0.245% 10 25.662 2239 2246 2257 rBV 1827044 3929987 99.33% 19.306%

11 30.730 2793 2798 2804 rBV 254205 491475 12.42% 2.414% 12 33.723 3115 3124 3136 rBV2 1204838 2831229 71.56% 13.908% 13 33.925 3142 3146 3153 rVB 27427 59895 1.51% 0.294% 14 36.156 3382 3389 3395 rBV 17506 51502 1.30% 0.253% 15 37.395 3518 3524 3538 rBV2 15680 57129 1.44% 0.281%

16 37.973 3579 3587 3609 rBV2 656589 1976292 49.95% 9.708% 17 38.855 3676 3683 3691 rBV5 13456 61517 1.55% 0.302%

Sum of corrected areas: 20356609

2561.D GCMS0308.M Thu Mar 21 14:17:10 2002

NYC-WTC_000038789

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NYC-WTC_000038789Source: NYC Law Department, mirrored locally

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