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DEP GCMS unknown compounds report, Mar 2002

Machine-extracted title · confidence 95%

GCMS analysis report dated March 6, 2002, listing other unknown compounds and surrogate recovery data for a different sample.

NYC-WTC_000003803–000003816

Folder label: “GCMS X 1/25/02 A 2/26/02

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NYC 9/11 Public Portal Document

Data . File : C:\HPCHEM\1\DATA\FEB2 502\1802.D Vial: 28 Acq On : 26 Feb 2002 4:31 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.320 787 793 806 rBV 526382 1374730 70.83% 13.783% 2 15.955 1183 1189 1203 rBV 823233 1832654 94.43% 18.374% 3 21.270 1762 1768 1784 rBV 925795 1940778 100.00% 19.458% 4 25.714 2246 2252 2265 rBV2 798380 1785508 92.00% 17.901% 5 30.790 2801 2805 2812 rVB 101373 202832 10.45% 2.034%

6 33.407 3085 3090 3096 rBV2 17394 39363 2.03% 0.395% 7 33.783 3124 3131 3150 rBV 563518 1315774 67.80% 13.191% 8 37.464 3525 3532 3539 rBV2 12735 45940 2.37% 0.461% 9 38.052 3588 3596 3612 rBV2 346685 1065073 54.88% 10.678% 10 38.942 3686 3693 3703 rBV2 18122 75837 3.91% 0.760%

11 40.751 3878 3890 3901 rBV4 20675 115921 5.97% 1.162% 12 42.973 4121 4132 4148 rBV3 17562 118006 6.08% 1.183% 13 45.782 4426 4438 4440 rBV3 14748 62010 3.20% 0.622%

Sum of corrected areas: 9974426

1802 .D GCMS0208.M Thu Feb 28 11:52:04 2002

NYC-WTC_000003808

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NYC-WTC_000003808Source: NYC Law Department, mirrored locally

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