GCMS analysis results for sample AE06799, April 2002

NYC 9/11 Public Portal Document ■— pY

Data File : C:\MSDCHEM\l\DATA\041602\6799.D Vial: 17 Acq On : 16 Apr 2002 9:48 pm Operator: Bohik Sample : SAMPLE 6799 3/21/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.43 4.51 ug/L 296218 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-31-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3] dioxolan-2-y... . 174 C8H14O4 000000-00-0 36 3 Pentanol, 5-amino- 103 C5H13NO 002508-29-4 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 400 (5.429 min): 6799.D (-) m/z 73.10 100.00% 73

5000 43 5.00 5.20 5.40 5.60 5.80

m/z-> 0 „lsl 7103........................ ‘ 0111—009—011101001111110111110121101100111—03111111117 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 m/z 43.10 26.63%

Abundance#36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 11T 5.00 5.20 5.40 5.60 5.80 43 m/z 45.10 7.38%

27 . 87 113TIWIWtg m/z-> 01 m T . 55 4 131 4-ri । > i 174 । ■ i > 11 ■ ■ ■ ■ । i-i < i 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 ...................- 5.00 5.20 5.40 5.60 5.80 5000 m/z 41.10 7.76%

43 27 55 87 113 131 174 0 ' I * ■ ‘h I‘‘‘lUEICEOO‘TCTETOTEICOEIT‘T m/z—> 20 30 40 50 60 70 80 90 100110 120 130 140150 16Q170 180 Abundance #9904: Pentanol, 5-amino- 33 Ai • > ■ > i ■ > • ■ i > 5.00 5.20 5.40 5.60 5.80 m/z 71.10 6.79%

5000

। 41 56 67 0 TDTTH TTTTTTggu 85 103 I.... i,,,,,,,, m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180 5.00 5.20 5.40 5.60 5.80

6799.D 5080402BBC.M Thu Apr 18 18:11:52 2002 Page 3

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