GCMS analysis results for sample AE06798, April 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\DATA\041602\6798.D Vial: 16 . Acq On : 16 Apr 2002 8:59 pm Operator: Bohik Sample : SAMPLE 6798 3/21/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.44 3.67 ug/L 263134 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 3 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 33 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 _______ 000994-05-8 33 Abundance Scan 401 (5.435 min): 6798.D (-) m/z 73.10 100.00%| 73

5000

43 5.00 5.20 5.40 5.60 5.80

m/z-> 0- —. Li—— 20___ 40 60 80 87 1Q3 100 120 140 160 180 m/z 43.10 22 .77%

Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 । , , 447 44 TPA 444 5.00 5.20 5.40 5.60 5.80 43 m/z 45.10 9.5 0%

27 0 ....... 44 55 _.... 87 113 1 i 1 ' • ' i ■ ■ ■ ■ i ' 1 ■ ■ i ' 1 131 174 m/z-> 20 40 60 80 100 120 140 160 180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $5 2-Cyclohexene-1-p... 73 — 5.00 5.20 5.40 5.60 5.80 5000 m/z 71.10 7.19%

43 1 27 : 55 0 > > । • i • > । ■ ■ TTpur 7 113 131 174 . m/z-> 20 40 60 80 100 120 140 160 180 Abundance #17063: 3-Pentanol, 2,4-dimethyl- — 73 5.00 5.20 5.40 5.60 5.80 1 i ■ '

m/z 41.05 6.97%

5000 55 43 27

m/z-> 15 0- 20 L 40 60 83 80 101 , 115.............. 100 120 140 160 180 IA lj|11 A' • A 5.00 5.20 5.40 5.60 5.80 ■ i ■ 1

5798.D 5080402BBC.M Thu Apr 18 18:05:32 2002 Page 3

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