GCMS analysis results for sample AE03383, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

..Data File : C:\MSDCHEM\1\DATA\032202\3383.D Vial: 41 Acq On : 22 Mar 2002 4:56 pm Operator: McLean Sample : 2/14/02 REINJ Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Acetic acid, 3-[l,3]dioxola... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.56 1.23 ug/L 739209 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetic acid, 3-[l,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 40 2 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 40 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 40 4 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 Abundance Scan 423 (5.565 min): 3383.D (-) m/z 73.20 100.00% 73

5000 43 ... ... T 5.20 5.40 5.60 5.80 6.00 0- _1______________ 1.1 55 tlIl, ~Iti . ll.l i ■ • ■ ■ i ■ • ■ ' T 1 ■ ‘ ' i • • 1 87193...... m/z 43.10 36.87% n/z-> 0 20 40 60 80 100 120 140 160 180 Abundance #78238: Acetic acid 3-[1,3]dioxolan-2-ylpropyl ester 73

5000 r PTTTTT sysaaummfr 5.20 5.40 5.60 5.80 6.00 43 m/z 45.10 13.99% 27 m/z—> 0^ 0 -5 20 40 60 87 113 131 TTTmnnBBTOTTTTTT 80 174 100 120 140 160 180 Abundance#36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $S 2-Cyclohexene-l-p... 73 . mm (1 5.20 5.40 5.60 5.80 6.00 5000 m/z 41.10 13.52%

43 27 55 87 113 131 174 0- ----- ■ • i • ■ ■ ■ । * > • • । • » * * । » । » * • • । • • • » । ' m/z-> 0 20 40 60 80 100 120 140 160 180 Abundance #4814: Silane, tetramethyl- 73 AAp4r 5.20 5.40 5.60 5.80 6.00 m/z 71.10 7.28%

5000

43 29 2 15 1.1 ' . 14, 0- ■ i ■ ■ • ■ i ■ 55 I r TT , 80 88 100 ‘ | • 1 ■ ■ ! ■ > • ■ | ‘ • t • > • ■ | • • • • | • TI T T 4 y /z—> 0 20 40 60 120 140 160 180 5.20 5.40 5.60 5.80 6.00

3383.D 5080302.M Mon Mar 25 09:43:02 2002 Page 3

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