GCMS analysis results for sample AE03076, March 2002

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Library Search Compound Report

. Data File : C:\MSDCHEM\1\DATA\031802\3076.D Vial: 7 Acq On : 19 Mar 2002 7:06 am Operator: McLean Sample : GC/MS SCAN 3/6 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.57 0.44 ug/L 125506 1,4-Dichlorobenzene-d4 9.55

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 9 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 9 3 3-Pentanol, 3-methyl- 102 C6H140 00007774-7 9 4 Acetaldehyde, O-methyloxime (CAS... 73 C3H7NO 033581-43-0 4 Abundance Scan 275 (5.570 mln): 3076.D (-) m/z 73.10 100.00% 73

5000

45 ‘I T Tr

m/z-> 0 .... 755 — T ■i 87 20 30 40 50 60 70 80 90 100110120130140150160170180 Trr 5.20 5.40 5.60 5.80 6.00 m/z 45.10 13.06%

Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cydohexene-1-p... 73

5000 '■i■ 5.20 5.40 5.60 5.80 6.00 43 m/z71.10 6.52%

m/z—> 0 . 27 . qmpm 55 m■i, > ■ । > i87I’ll i >« i j 11 >>113 [>’•< i 20 30 40 50 60 70 80 90 100110120130140150160170180 131 174

Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-yipropyl ester 73 ‘*‘*I**‘‘I‘ 5.20 5.40 5.60 5.80 6.00 5000 m/z55.10 6.49%

43 27 0 pmttm 55 T . , 87 113 131 174 ‘ ‘ • I ■'111 ‘' '■’T ‘‘ FTi p i ■ 111 ■ 11111111111 n >> i > । ■ 111111 m/z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #9665:3-Pentanol, 3-methyl- 73 • i ■ • ■ ■ i ■ • ■ ■ i 5.20 5.40 5.60 5.80 6.00 1' I ■1 ■ ■ i •

m/z 69.10 4.05%

5000 55 43 87 29 0-mmmh ‘ l • • • ■ l1 ■ ■ > i • • • ■ i ■ Tl/Z-> 20 30 40 50 60 70 80 90 100110120130140150160170180 5.20 5.40 5.60 5.80 6.00

3076.D 5080302.M Tue Mar 19 21:33:30 2002 Page 3

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