Laboratory data recording surrogate recovery and unknown compound screening for sample AE04514 dated April 4, 2002.
NYC-WTC_000038703–000038711Folder label: “GCMS X 3/2/02 A 3/27/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\032602\4514.D Vial: 59 - Acq On : 27 Mar 2002 9:40 pm Operator: McLean Sample : SAMPLE 4514 3/2/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Acetic acid, 3-[1,3]dioxola... Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
5.58 0.54 ug/L 142051 1,4-Dichlorobenzene-d4 9.55
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 50 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL 174 C8H14O4 015745-87-6 50 3 1,3-Dioxolane 74 C3H6O2 000646-06-0 9 4 1,3-Dioxolane (CAS) $$ 1,3-Dioxo... 74 C3H602 000646-06-0 9 Abundance Scan 425 (5.576 min): 4514.D (-) m/ z 73.20 100.00% 73
5000 43 ■ । • ■ ■ ■ । ■ TTTTPMI’r 5.20 5.40 5.60 5.80 6.00 1 55 i 103 ............. — 87 m/z 43.20 36.89% 0 H..... mm m/z->___ 20 30 40 50 60 70 80 90 100110120130140150160170180 r "' r ■
Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73
5000 W X 4 A AM A 4AAA [ I ! I t | I I I I | I 5.20 5.40 5.60 5.80 6.00 m/z 41.10 15.80% 43 27 55 ,l 87 113 131 174 m/z-> 0 -- Ir ' ■ TT Hm " ।1 TTTTmtrT 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance#36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70 4 4.. 5.20 5.40 5.60 5.80 6.00 m/z 45.10 14.70% 5000
43 27 87 0 T 55 r " ‘IT' ■i''1■i'■'' i ■'' 'i113 131 174 '''' i ■'''i'’''i'''' i'''' i'' ■' i •'''i'' m/z—> 20 30 40 50 60 70 80 90 100110120130140150160170180 Abundance #1996: 1,3-Dioxolane 70 5.20 5.40 5.60 5.80 6.00 m/z 71.10 8.67%
5000 44
29
m/z-> 0 mH Th 57 |‘ " 1 | ’ 1] I’T 20 30 40 50 60 70 80 90 100110120130140150160170180 i•■■‘i I' I ■ । ■ i ■ • L.. 5.20 5.40 5.60 5.80 6.00
4514.D 5080302.M Thu Mar 28 06:24:41 2002 Page 3
NYC-WTC_000038710
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NYC-WTC_000038721
Laboratory data recording surrogate recovery and unknown compound screening for sample AE04512 dated April 4, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039254
Analytical data for sample AE03270 showing detection of unknown compounds and surrogate recovery on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038949
Laboratory report documenting GCMS analysis of sample AE02094 conducted on March 20, 2002, showing surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039237
Analytical data for sample AE08268 showing detection of unknown compounds and surrogate recovery on March 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039262
Gas chromatography-mass spectrometry analysis of sample AE06271 performed March 22, 2002, detecting unknown compounds and 2,4-DDD surrogate at 5.0 ug/L.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059066
Laboratory report documenting GCMS analysis of sample AE05240 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059084
Laboratory report documenting GCMS analysis of sample AE05242 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059048
GCMS analysis of sample AE05238 performed on 3/29/02 showing 2,4-DDD surrogate compound recovery at 152% with unspecified qualifier flag.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059075
Laboratory report documenting GCMS analysis of sample AE05241 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000012453
Gas chromatography-mass spectrometry results for sample AE04379 analyzed on April 2, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059057
Laboratory report documenting GCMS analysis of sample AE05239 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011635
Gas chromatography-mass spectrometry analysis report for sample AE03475 identifying other unknown compounds, conducted March 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000038657
Department of Environmental Protection site log sheet for the World Trade Center area dated March 2002.
Filed in the same folder
NYC-WTC_000038658
Laboratory data sheet recording sample volumes and drip rates for DEP analysis in early March 2002.
Filed in the same folder
NYC-WTC_000038661
Gas chromatography-mass spectrometry analysis report for environmental sample AE04509 dated March 27-28, 2002.
Filed in the same folder
NYC-WTC_000038670
Calibration data for GCMS analysis of volatile organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000038678
Blank analysis results showing no detectable levels of target volatile organic compounds in sample AE04509.
Filed in the same folder