GCMS blank analysis results for sample AE06795, April 2002

NYC 9/11 Public Portal Document 7 ~pouliu RCpUL L

Data File : C:\MSDCHEM\l\DATA\041602\6795.D Vial: 13 Acq On : 16 Apr 2002 6:31 pm Operator: Bohik * Sample : SAMPLE 6795 3/21/02 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 1,3-Dioxolane, 2-pentadecyl... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.44 7.53 ug/L 575173 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-pentadecyl- $$ ... 284 C18H36O2 004360-57-0 38 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 3 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 4 1,3-Dioxolane, 2-methyl- (CAS) $... 88 C4H8O2 000497-26-7 9 Abundance Scan 401 (5.435 min): 6795.D (-) m/z 73.10 100.00% 73

5000

43 5.00 5.20 5.40 5.60 5.80 0 —58 4 । 88 103...... m/z 43.10 22.52% m/z—> 20 40 60 80 100 120 140 160 180 200220 240 260 280 Abundance #231414: 1,3-Dioxolane, 2-pentadecyl- $$ Hexadecanal cycii... 73

5000 — 5.00 5.20 5.40 5.60 5.80 m/z 45.10 8.98%

m/z—> 0 L27 ..11 .58.— 99 115 137152167183 222 240256 283 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... I 73 A 5.00 5.20 5.40 5.60 5.80 5000 m/z 41.20 8.33%

43 27 I 88 113 131 174 0- __■ • ___ j i > ■ ■ m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 — 'Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyi ester 73 —MM 5.00 5.20 5.40 5.60 5.80 m/z 71.10 6.85%

5000

43 27 m/z—> 0+4 —T * 20 40 48 ' i''113" i'131 174 " ' I'1 " 11 " 1111 " I i' " 11 — A—— 60 80 100 120 140 160 180 200 220 240 260 280 5.00 5.20 5.40 5.60 5.80

795.D 5080402BBC.M Thu Apr 18 16:3-0:38 2002 Page 3

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