GCMS analysis results for sample AE06591, April 18, 2002

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Laboratory report documenting GCMS analysis of environmental sample AE06591 conducted on April 18, 2002.

NYC-WTC_000039857–000039865

Folder label: “GCMS X 3/20/02 A 4/15/02”

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NYC 9/11 Public Portal Document

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* Data File : C:\MSDCHEM\l\DATA\041502\6591.D Vial: 18 Acg On : 16 Apr 2002 12:02 am Operator: Bohlk Sample : SAMPLE 6591 3/20/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 1,3-Dioxolane, 2-pentadecyl... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.42 12.10 ug/L 820194 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane, 2-pentadecyl- $$ ... 284 C18H36O2 004360-57-0 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 28 Abundance Scan 399 (5.423 min): 6591.D (-) m/z 73.10 100.00% 73

5000

43 i ' ■ ■ ' i ‘ 5.00 5.20 5.40 5.60 5.80 _5888103 0 । ■ ■ ■ ■ T’' ■ ■ i ■ 11 i'1" i ■" ■ i ■ ■ ■ ■ i" ■ ■ i ■ ‘" i ■ ■ ■ ■ i' ■ • ■ i" ■ ■ i • ■ ■ ‘ i" ■ ■ i ■ ■ m/z 43.10 22.45% m/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 #231414: 1,3-Dioxolane, 2-pentadecyi- $$ Hexadecanal cycli... I 73

5000 I " " I f‘ ' TTIT11 5.00 5.20 5.40 5.60 5.80 m/z 45.10 9.46%

m/z—> 0 27.41,58... 99 115 137152167183 222 240256 283 'I ■1 ■ ■ i'‘■ ■ i ■' " i" ■' i ■' ■ ■ i " ■' i " '' i'' ■ ■ i ■1'' i1'' 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #78238: Acetic acid, 3-[1 ,3]dioxolan-2-ylpropyl ester __________________ 73

5.00 5.20 5.40 5.60 5.80 5000 m/z 41.10 8.22%

27 88 174 113 131 o — ■I' ■1■ I’’T "1’’’11"""111111111111111101ETEITUTTTTIIITTT m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 i' 11 ' i ' ' k - —44 AA— 5.00 5.20 5.40 5.60 5.80 m/z 71.10 6.75%

5000

27 0 ,,, , . 88 113 131 174 T i'' " i ‘1' ' i " " 111'11 ''i' " i " " i'' ■■ i 11 11 ■ ...............1 —44 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 5.00 5.20 5.40 5.60 5.80

6591.D 5080402BBC.M Wed Apr 17 18:09:26 2002 Page 3

NYC-WTC_000039864

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NYC-WTC_000039864Source: NYC Law Department, mirrored locally

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