GCMS analysis results for sample AE06588, April 18, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\041502\6588.D Vial: 12 Acq On : 15 Apr 2002 7:06 pm Operator: Bohik Sample : SAMPLE 6588 3/20/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.43 11.05 ug/L 794546 1,4-Dichlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 33 2 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 3 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 9 4 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 9 Abundance Scan 400 (5.429 min): 6588.D (-) m/z 73.10 100.00% 73

5000

43 —।। i . । . । । । i । । > । । ' |T~i । । । । i । 5.00 5.20 5.40 5.60 5.80

m/z—> 0 ' 1 i ■ 20 —1 AX 41 40 60 80 87 103 100 120 140 160 180 m/z 43.10 22.35%

Abundance #9702: Butane, 2-methoxy-2-methyl-S$ Ether, methyl tert-p... 73

5000 TTTTTTg PT’* 5.00 5.20 5.40 5.60 5.80 43 55 87 m/z 45.10 9.53% 29

fn/z-> 0- ...... 20 4—40 "II 60 TIT 80 100 120 140 160 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 30 73 i ' ' ■ ■ i ' ' ' i • ■ 5.00 5.20 5.40 5.60 5.80 5000 m/ z 41.10 8.25%

44 58

18 0 ' 1 i ' ' i ' ' ' ' i ' ' ' ' i ' ■ ■ • .................................. ... ‘ ■ i ■ m/z-> 20 60 80 100 120 140 160 180 Abundance#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 —44 A— Am— 5.00 5.20 5.40 5.60 5.80 m/z 71.10 7.24%

5000

43

0 - 44 1 I ■ > 55 27 * ■ । , », j J, 87... 113 131...... 174 , — m/z-> 20 40 60 80 10C 120 140 160 180 5.00 5.20 5.40 5.60 5.80

6588.D 5080402BBC.M Wed Apr 17 17:46:54 2002 Page 3

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