GCMS analysis results for sample AE08954, April 29 2002

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Data File : C:\MSDCHEM\1\DATA\042202\8954.D Vial: 16 Acq On : 22 Apr 2002 11:27 pm Operator: Bohik Sample : SAMPLE 8954 4/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 1 Butane, 2-methoxy-2-methyl-... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

5.47 0.85 ug/L 65755 1,4-Diehlorobenzene-d4 9.41 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 38 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 9 Abundance Scan 407 (5.470 min): 8954.D (-) m/z 73.10 100.00% 73

5000' 43 ■ • i' ■ ■ ■ i TTTTTTTT 5.20 5.40 5.60 5.80 5155 59 69 87 m/z-> 0 mhhmdmm TpTTHTTTTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 43.10 26.56%

Abundance #9702: Butene, 2-methoxy-2-methyl- $$ Ether, methyl tert-p... 73

5000 43 5.20 5.40 5.60 5.80’ 55 87 m/z 45.10 11.82% 29

n/z-> 0 ’ICEETETT 1 33 1111H1!. 1111 rrrTTtr rIJ!11111 >i> 150 ,i,11,39 Wpgr 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 „59..789l +8%m7 Abundance #9665:3-Pentanol, 3-methyl- 73 • ■ j • । >11 i ‘ j i * • 5.20 5.40 5.60 5.80 5000 m/z 41.10 11.14% 55 43 87 69 29 39 51 .,59 | 0, •i” " r‘‘'i 11111,11111111 [ 11 miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 4) —AM*** 5.20 5.40 5.60 5.80 73 m/z71.10 9.66%

5000 44 58

18 2 /z—> 0 +44 54 TI pmh I 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 p T 5.20 5.40 5.60 5.80 T

8954.D 5080402BBC.M Fri Apr 26 12:04:35 2002 Page 3

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