GCMS analysis results for sample AE06588, April 18, 2002

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Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\041502\6588.D Vial: 12 Acq On : 15 Apr 2002 7:06 pm Operator: Bohik Sample : SAMPLE 6588 3/20/02 Inst Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Library : C:\DATABASE\WILEY7N.L

Peak Number 2 4,10-Dioxatrideca-1,6,12-tr... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

10.25 0.88 ug/L 62976 1,4-Di chlorobenzene-d4 9.41

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4,10-Dioxatrideca- 1,6,12-triyne ... 176 C11H12O2 117911-56-5 17 2 2-Amino-4-hydroxypyrrolo[2,3-d]p... 150 C6H6N4O 000000-00-0 9 3 Dezaguanine $$ ICN 4221 $$ 3-Dea... 150 C6H6N4O 041729-52-6 9 4 Tricyclo[3.3.1.1(3,7)]decanone (... 150 C10H14O _____ 000700-58-3 9 Abundance Scan 1221 (10.253 min): 6588.D (-) m/z 150.00 100.00% 150

5000 52 115 78 T ' I T’ T’I r • r ‘T AAA, 40 87 10.00 10.20 10.40 10.60 m/z 152.00 62.02% 0 " i' ■ "II——III01111111T m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #81073: 4,10-Dioxatrideca-1,6,12-triyne $$ 2-Pentyne, 1,5-... 39

79 91 107

5000 69 52 10.00 10.20 10.40 10.60 117 m/z 52.10 35.51%

| 176 0- TCBO—NOgur m/z-> 30 40 50 60 70 80 90 100 110 120 130140150160170 180 Abundance #45711: 2-Amino-4-hydroxypyrrolo[2,3-d]pyrimidine 150 43

10.00 10.20 10.40 10.60 5000 m/z 115.05 34.73% 52 133 80 108

m/z-> 0- TIT — 44 94 II 121 j TOggTT 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 1' ‘ ■ i'' ■ ■ i ■''' i ■'

Abundance #45713: Dezaguanine $$ ICN 4221 $$ 3-Deazaguanine $$ 4H-lm... 150 . . । . ■ ■ i ' ' 10.00 10.20 10.40 10.60 m/z 78.10 29.15%

5000 43 52 105 133 78 6895 122

m/z-> 0 +4+ -mm 1... 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 10.00 10.20 10.40 10.60

5588. D 5080402BBC.M Wed Apr 17 17:46:55 2002 Page 4

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