Laboratory report documenting GCMS analysis of sample AE06455 conducted on April 19, 2002, by the DEP.
NYC-WTC_000039588–000039610Folder label: “GCMS X 3/19/02 A 4/17/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6455 . D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 12 Noradrenaline, tetra-TMS Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 29.19 0.49 ug/1 71690 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 25 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 3 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 17 4 3-IsopropQxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 17 Abundance Scan 2630 (29.187 min): 6455.D (-) m/ z 73.00 100.00%l 73
5000 147 355 221 ----- 281 1 i ' 1 28.80 29.00 29.20 29.40 29.60 327 mz-> 45 TTTg] । —... 191 4+ 401 429 TT. tt T TTT J ", >pi ii11i*i11(11 40 60 80 100120140160180200220240260280300320340360380400420440 m/z 147.00 37.98% Abundance #57357: Noradrenaline, tetra-TMS 73
5000 102 355 ‘I ■ 1 i 1 1 28.80 29.00 29.20 29.40 29.60 m/z 355.05 33.70% 45 147 442 I i ′ •" i1" * r TT I "'' I i" " r "111"' i" " 111" i1"111" ’i T‘TTT‘11T m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 1 I I I I I I I I T I T I 281 28.80 29.00 29.20 29.40 29.60 5000- m/z 220.95 26.54%
369 ‘T 111 " I I‘‘‘IT 207 249. ( 338 | r1" i1' “ I,T" r • ■' i" “ {11 •' p"111 ‘111 TTIT]i1111111111" ■' r m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet ' ' i ' 1 1 1 i ' 1 73 355 28.80 29.00 29.20 29.40 29.60 m/z 281.00 20.71% 5000
147 267
m/z—> 47 TTT L U‘EIEE-EE"0‘7UT T'"11 208 237 I L ll i TTTT ■ ■ ‘i'"■ i11'1 r "'I I " ’' I 40 60 80 100120140160180200220240260280300320340360380400 420 440 i"" i i —r । ।—।—।—PP --- 28,80 29.00 29.20 29.40 29.60
6455.D GCMS0412.M Thu Apr 18 09:14:23 2002 Page 12
NYC-WTC_000039606
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000039497
Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039469
Laboratory report documenting GCMS analysis of sample AE06430 conducted on April 19, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038871
Laboratory report documenting GCMS analysis of sample AE02575 conducted on March 25, 2002, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039611
Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039560
Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039574
Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005394
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02604.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000005415
Laboratory report listing unknown compounds and surrogate recovery data for sample AE02645.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009835
Calibration data for GCMS analysis using 625/TCLP method with deuterated compound reference standards recorded on February 21, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000023789
Instrument log and analysis summary for GCMS testing of sample AE09676 conducted on May 23, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047979
GCMS analysis report for sample AE05749 showing surrogate recovery and unknown compounds from April 2002.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000060478
DEP laboratory report of GCMS analysis for sample AE06635 conducted on April 18, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000039437
Department of Environmental Protection site log sheet for the World Trade Center area covering March and April 2002.
Filed in the same folder
NYC-WTC_000039438
Fragmented page from a GCMS record series dated April 2002 within DEP Box 23 archives.
Filed in the same folder
NYC-WTC_000039441
Calibration report for GCMS analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039445
Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder
NYC-WTC_000039453
Laboratory report documenting GCMS blank analysis of sample AE06430 conducted on April 17, 2002.
Filed in the same folder