GCMS analysis results for sample AE06430, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\APR1702\6430.D Vial: 6 Acq On : 17 Apr 2002 1:08 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 13 Benzoic acid, 2,6-bis[(trimeth Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 29.19 0.78 ug/1 129886 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 16 2 Noradrenaline, etra-TMS 457 C20H43NO3Si4 000000-00-0 16 3 3 - Isopropoxy-1,/1 / 1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 16 4 Benzoic acid, ,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 14 Abundance Scan 2630 (29.186 min): 6430.D (-) m/ z 73.00 100.00% 73

5000 147 355 221 - 281 28.80 29.00 29.20 29.40 29.60 45 117 191[ , 249 i , 327, I 401 429 Tnm 4 11 1 1 1 * 1 > ■ i ■ • ■ 1 14 “ t ■ ' 1—1—ITTTT m/z 147.00 43.10% miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51296: Benzoic acid, 2,6-bis[(trimethylsilyl)oxy]-, trimet 73 355

5000 "I l ■ i 1 ■ 28.80 29 00 29 20 29.40 29.60 147 267 m/z 355.05 35.29% 47 . Il 208 237 | miz—> 50 100 - I * ' 1 ) 1 —' 150 200 250 300 350 400 450 500 550 Abundance #57357: Noradrenaline, tetra-TMS 73 ■ i ' 1 1 1 i ‘ ' I ■ ■ i ■ ■ - ■ i ■ ■

28.80 29.00 29.20 29.40 29.60 5000 102 355 m/Z 221.05 29.46%

45 | 147 442 m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73 11 1 1 I 1 1 1 1 I 1 1 28.80 29.00 29.20 29.40 29.60 m/Z 281.10 22.40% 5000 147

221 281 327 I ■ ■ i ■ ■ ■ < i ■ ■ ' > । ■ 415 519 561 1 ' i 1 ‘ 1 1 i ■ ■ 1 1 1 1 1 1 1 1 1 ... 4..... , m/z—> 50 100 150 200 250 300 350 400 450 500 550 28.80 29.00 29.20 29.40 29.60

6430.D GCMS0412.M Thu Apr 18 09:09:30 2002 Page 13

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