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GCMS analysis results for sample AE06449, April 2002

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Laboratory report documenting GCMS analysis of sample AE06449 conducted on April 19, 2002.

NYC-WTC_000039497–000039521

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C : \HPCHEM\ 1 \DATA\ APRI7 02\6449.D Vial: 7 Acq On : 17 Apr 2002 2:06 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Noradrenaline, tetra-TMS Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 29.19 0.49 ug/1 84439 Phenanthrene-dl0 25.58 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 32 2 Trisiloxane, 1,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 27 3 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 27 4 3-Isopropoxy-1/, 1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 Abundance Scan 2630 (29.193 min): 6449.D (-) m/z 73.00 100.00* 73

5000 147 355 221 281 i 1 1 ‘ 1 i ■ ' ‘t[/1/1/1111/1/1/11/—.T 28.80 29.00 29.20 29.40 29.60 45 i. _ 191 |........ _ 327, ( 401 429 . । f 111 j. r1.11111 ]... 11 1′11101-11—01101111 11'" ।11 *' i I l i l I TTI i i Tj TTTTTTTTTTTTTTTT m/z 355.05 43.20% m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #57357: Noradrenaline, tetra-TMS 73

5000 102 355 T[ 28.80 29.00 29.20 29.40 29.60 m/z 147.00 43.12% 45 147 442 I I. I ' i ■"11" " i" " "11 ln"I i ”11 r ■'11" " i" " i11 ■11 l""l I n/z--> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #52459: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 147 -............... 281 28.80 29.00 29.20 29.40 29.60 5000 m/z 221.05 31.88%

369 207 249 I, 338 1, TT I''" I u " I " " I TTTTTTTT 11111111 ’ ■ i"'1 r n ■ iI ""I •' "I" " I m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 28.80 29.00 29.20 29.40 29.60 m/z 281.00 26.12%! 355 267 5000

207 323 , ................ .. TT’ I'" ■ J " " I in. I.... I.... I TV* I" " I T0TT I ’"'I 11 1 1 ' 1 1 I 1 1 1 1 I1 1 1 113 । । । । । । m/z—> 40 60 80 100120140160180200220240260280 300 320 340 360 380 400 420440 28.80 29.00 29.20 29.40 29.60

6449.D GCMS0412.M Thu Apr 18 09:10:54 2002 Page 11

NYC-WTC_000039514

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NYC-WTC_000039514Source: NYC Law Department, mirrored locally

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