GCMS results for sample AE08935, April 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR2302\8935.D Vial: 15 Acq On : 24 Apr 2002 4:03 am Operator: Sample : gc/ms scan 4/15 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.81 0.31 ug/1 53356 Naphthalene-d8 15.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H30O5Si5 000541-02-6(87 2 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-037 3 N-(Trifluoroacetyl)-N,O,O',0 ''-tetr 553 C22H42F3NO4Si4 000000-00-0 37 4 Phenethyls tine, N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1063 (14.807 min): 8935.D (-) m/z 73.00 100.00% 73

5000 267 355 ........ 14.40 14.60 14.80 15.00 15.20 45 154 191 —■

m/z->____ 50 100 i ■ ■

150 200 11111323, 250 300 350 400 450 ............................... .. ■ ■ m/z 267.00 500 550 | 44.21% Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/ z 355.05 41.25% 207 323 TI—k —11PP miz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #57357: Noradrenaline, tetra-TMS 73 ......................... I 1 ' 1 1 I ‘ ‘ ' J ' ‘ 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 15.03% 102

45 I 147 ........................................................... 442.......................... miz-s 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-OTrifluoroacetyll-N.O.O'.OMetrakisCrimethylsi i ■ ■ ‘ ■ i ■ ■ ■ • i ' ‘ i ■ ■ ■ ■ i ■ ' 73 14.40 14.60 14.80 15100 15.20 m/z 267.90 12.55% 355 5000

45 1 it 147 193 267 538 .................... M....................... • ‘ 1 1 * * * 1 * 1 * ’ I ‘ ' *■ I ’ ‘ ‘ ’ I ‘ ‘ i ' ■ ■ ■ i ' ■ ■ ■ i 1 ■ • ■ I ■ 1 • ■ i ' 1 miz—> 50 100 150 200 250 300 350 400 450 500 550 I 14.40 14.60 14.80 15.00 15.20

8935.D GCMS0412.M Wed Apr 24 08:39:10 2002 Page 2

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