GCMS analysis results for sample AE06455, April 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6455.D Vial: 13 Acq On : 17 Apr 2002 7:57 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 11 1-Monolinoleoylglycerol trimet Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 27.42 0.63 ug/1 92170 Phenanthrene-dl0 25.59 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Monolinoleoylglycerol trimethylsi 498 C27H5404Si2 054284-45-6 36 2 3-Isopropoxy-1,1,1,7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 3 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 25 4 Tris iloxane, 1/1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 25 Abundance Scan 2438 (27.424 min): 6455.D (-) m/ z 73.00 100.00% 73 A

5000 147 221 281 355 42Q 27.00 27.20 27.40 27.60 27.80 45 117 1911 _ 249 327, [ 401 71 ■ ■'i '■ ■ TT T T 11 I ' m/z 147.00 41.77%| m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58871:1 -Monolinoleoylglycerol trimethylsilyl ether 73

207 ........ / ' 5000 147 r■ 1 ■ ’ । 1 ' • ■ । 1 27.00 27.20 27.40 27.60 27.80 34 103 m/z 281.10 25.64% । — 281

m/z-> 50 100 . , , , 325 — 482 4 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-Isopropoxy-1 ,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

27.00 27.20 27.40 27.60 27.80 5000 m/z 221.05 24.96%| 147

221 21 327 415 519 561 ■ ■ । • 1 । ■ 1 ■ i ' 1 1 1 I ■ 1 1 1 i 1 1 1 1 i ■ "■ ■ ■ i ■ ’ m/z—> 50 100 150 200 250 300 350 400 450 500 550 Abundance #30580: Ethanedioic acid, bis(trimethylsilyl l) ester 73 147 27.00 27.20 27.40 27.60 27.80 m/z 355.05 11.53%| 5000 45

| 190 219 m/z-> — 50 ll—100 —- 150 200 250 300 350 400 450 500 550 I ' 1 1 1 i ■ 1 1 1 i ■ ' [ ' i ' 1 1 "I—T 27.00 27.20 27.40 27.60 27.80

6455.D GCMS0412.M Thu Apr 18 09:14:22 2002 Page 11

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