GCMS analysis results for sample AE06456, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE06456 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039611–000039627

Folder label: “GCMS X 3/19/02 A 4/17/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1702\6456.D Vial: 14 Acq On : 17 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 3/19 fb Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P ■ Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 36.09 1.64 ug/1 128465 Perylene-dl2 37.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,1,5,7,7,7 Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 28 2 Trisiloxane, ,1,1,5,5,5-hexamethyl 384 C12H3604Si5 003555-47-3 22 3 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 12 4 Noradrenaline, tetra-TMS____________ 457 C20H43NO3Si4 000000-00-0 10 Abundance I Scan 3382 (36.090 min): 6456. D (-) m/z 73.00 100.00% 73

147 5000 221 281 355 429 35.80 36.00 36.20 36.40 44 117 TEITEEUOTTTTT 193 . ""i1'"I 253 । i " " i11 4.. 327— — 401 . i1" 11" " i11" r "11"" i " 1111'I''111 m/z 147.00 62.45% m/z-> 40 60 80 100120140160180 200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73

147 5000 267 TT1 355 429 35.80 36.00 36 20 36.40 45 207 m/z 221.05 48.87% TWIT “ r "11" ■ ‘ i ■"11" " i ■" ■ r TTTTTT L TTT . . M | . >> I | H 1 . | . 1%. | m/z—> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #74103: Trisiloxane, 1,1,1,5,5,5-hexamethyl-3,3-bis[(trimet 73 -- 147 35.80 36.00 36.20 36.40 | 5000 m/z 355.05 30.90% 281 45 369 I i"' 'I ......... 117..... ,........... i " " r " ‘ i'" ‘ i" r1" i 207 TTT—_____ Tu 11111111111111 mlz-> 40 60 80 100120140160180 2CXj 220 240 260 280 300 320 340 360 380 400 420 Abundance #56734:3-Trimethylsilyloxystearic acid, trimethylsilyl est ■ ■ i ■ ■ ■ ■ i • 1 * i ■ 11 1 i * • 73 35.80 36.00 36.20 36.40 m/z 281.00 27.21% 5000 147 233

313 429 189

mtz-> r1 "i " "i""i""r111''I" I"1'...... 1 | 339 i1i" " i'1111"'11'V " • i •i1'111 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 387 X 11"11 35.BP 36.00 36.20 36.40

6456.D GCMS0412.M Thu Apr 18 09:15:06 2002 Page 4

NYC-WTC_000039621

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000039621Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS analysis results for sample AE06452, April 2002 · Box DEP Box 23

NYC-WTC_000039545

Laboratory report documenting GCMS analysis of sample AE06452 conducted on April 19, 2002, by the DEP.

1 shared topics · Same agency, volume and box · similarity 0.998